4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-3-iodo-β-D-mannopyranose

Base Information

Chemical Name:4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-3-iodo-β-D-mannopyranose
CAS No.:92982-54-2
Molecular Formula:C₁₆H₁₈INO₆
Molecular Weight:447.227
Hs Code.:

Synonyms:4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-3-iodo-β-D-mannopyranose

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Chemical Property of 4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-3-iodo-β-D-mannopyranose

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Technology Process of 4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-3-iodo-β-D-mannopyranose

There total 6 articles about 4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-3-iodo-β-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72503-88-9
2-amino-1,6-anhydro-2-deoxy-β-D-mannopyranose

: 92982-54-2
4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-3-iodo-β-D-mannopyranose

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / pyridine / 1.) -15 deg C, 2.) room temperature

2: 64 percent / pyridine / Ambient temperature

3: 80 percent / sodium methoxide / CHCl₃; methanol / 1 h / Ambient temperature

4: 1.1 g / sodium iodide / acetic acid / 0.08 h / 80 °C

5: pyridine / Ambient temperature

With pyridine; sodium methylate; sodium iodide; In methanol; chloroform; acetic acid;
DOI:10.1016/0008-6215(84)85273-8

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 92982-54-2
4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-3-iodo-β-D-mannopyranose

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / pyridine / 1.) -15 deg C, 2.) room temperature

2: 64 percent / pyridine / Ambient temperature

3: 80 percent / sodium methoxide / CHCl₃; methanol / 1 h / Ambient temperature

4: 1.1 g / sodium iodide / acetic acid / 0.08 h / 80 °C

5: pyridine / Ambient temperature

With pyridine; sodium methylate; sodium iodide; In methanol; chloroform; acetic acid;
DOI:10.1016/0008-6215(84)85273-8

Reference yield:

: 92982-53-1
1,6:3,4-dianhydro-2-benzyloxycarbonylamino-2-deoxy-β-D-altropyranose

: 92982-54-2
4-O-acetyl-1,6-anhydro-2-benzyloxycarbonylamino-2,3-dideoxy-3-iodo-β-D-mannopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 1.1 g / sodium iodide / acetic acid / 0.08 h / 80 °C

2: pyridine / Ambient temperature

With pyridine; sodium iodide; In acetic acid;
DOI:10.1016/0008-6215(84)85273-8