tert-butyl N-[1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-1-(phenylsulfonyl)methyl]carbamate

Base Information

Chemical Name:tert-butyl N-[1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-1-(phenylsulfonyl)methyl]carbamate
CAS No.:934768-45-3
Molecular Formula:C₁₇H₂₅NO₆S
Molecular Weight:371.455
Hs Code.:

Synonyms:tert-butyl N-[1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-1-(phenylsulfonyl)methyl]carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl N-[1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-1-(phenylsulfonyl)methyl]carbamate

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Technology Process of tert-butyl N-[1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-1-(phenylsulfonyl)methyl]carbamate

There total 1 articles about tert-butyl N-[1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-1-(phenylsulfonyl)methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 4248-19-5
tert-butyl carbazate

: 618-41-7
Benzenesulfinic acid

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 934768-45-3
tert-butyl N-[1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-1-(phenylsulfonyl)methyl]carbamate

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/b309211a

Reference yield:

: 934768-45-3
tert-butyl N-[1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-1-(phenylsulfonyl)methyl]carbamate

: 4-(2,2-dimethyl-[1,3]dioxolan-4-yl)-5-vinyl-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / Zn / dimethylformamide / 2 h / 20 °C

2: K₂CO₃ / methanol; H₂O / 2 h / 20 °C

3: NaH / dimethylformamide / 20 °C

With sodium hydride; potassium carbonate; zinc; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo062265n

Reference yield:

: 934768-45-3
tert-butyl N-[1-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-1-(phenylsulfonyl)methyl]carbamate

: 784191-96-4
(4S,5S)-4-[(4S)-2,2-dimethyl-1,3-dioxolan-4-yl]-5-vinyl-1,3-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / Zn / dimethylformamide / 2 h / 20 °C

2: K₂CO₃ / methanol; H₂O / 2 h / 20 °C

3: NaH / dimethylformamide / 20 °C

With sodium hydride; potassium carbonate; zinc; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo062265n