2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-O-acetyl-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

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Chemical Name:2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-O-acetyl-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole
CAS No.:1330667-43-0
Molecular Formula:C₁₈H₁₇ClF₃N₃O₅S
Molecular Weight:479.864
Hs Code.:

Synonyms:2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-O-acetyl-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

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Chemical Property of 2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-O-acetyl-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

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Technology Process of 2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-O-acetyl-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

There total 3 articles about 2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-O-acetyl-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1628180-78-8
C₁₈H₁₉ClF₃N₃O₅S

: 1330667-43-0
2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-O-acetyl-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

Guidance literature:: With manganese(IV) oxide; In chloroform; for 1h;
DOI:10.3390/molecules19067832

Reference yield:

: 38901-30-3
4-[4-chloro-3-(trifluoromethyl)phenyl]-3-thiosemicarbazide

: 1330667-43-0
2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-O-acetyl-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 6 h / Reflux

2: manganese(IV) oxide / chloroform / 1 h

With manganese(IV) oxide; In dichloromethane; chloroform;
DOI:10.3390/molecules19067832

Reference yield:

: 24807-97-4
3-O-acetyl-1,2-O-isopropylidene-α-D-xylo-pentodialdo-1,4-furanose

: 1330667-43-0
2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-O-acetyl-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 6 h / Reflux

2: manganese(IV) oxide / chloroform / 1 h

With manganese(IV) oxide; In dichloromethane; chloroform;
DOI:10.3390/molecules19067832