2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

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Chemical Name:2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole
CAS No.:1628180-91-5
Molecular Formula:C₁₆H₁₅ClF₃N₃O₄S
Molecular Weight:437.827
Hs Code.:

Synonyms:2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

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Chemical Property of 2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

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Technology Process of 2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

There total 4 articles about 2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1330667-43-0
2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-O-acetyl-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

: 1628180-91-5
2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 0.5h;
DOI:10.3390/molecules19067832

Reference yield:

: 38901-30-3
4-[4-chloro-3-(trifluoromethyl)phenyl]-3-thiosemicarbazide

: 1628180-91-5
2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 6 h / Reflux

2: manganese(IV) oxide / chloroform / 1 h

3: sodium methylate / methanol / 0.5 h / 20 °C

With manganese(IV) oxide; sodium methylate; In methanol; dichloromethane; chloroform;
DOI:10.3390/molecules19067832

Reference yield:

: 24807-97-4
3-O-acetyl-1,2-O-isopropylidene-α-D-xylo-pentodialdo-1,4-furanose

: 1628180-91-5
2-(4-chloro-3-(trifluoromethyl)phenylamino)-5-(2R,3R-O-isopropylidene-4R-tetrahydrofuro-2,3,4-triol-5S)-1,3,4-thiadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 6 h / Reflux

2: manganese(IV) oxide / chloroform / 1 h

3: sodium methylate / methanol / 0.5 h / 20 °C

With manganese(IV) oxide; sodium methylate; In methanol; dichloromethane; chloroform;
DOI:10.3390/molecules19067832