2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl tert-butyldimethylsilylether

Base Information

Chemical Name:2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl tert-butyldimethylsilylether
CAS No.:174867-47-1
Molecular Formula:C₂₄H₃₆O₃Si
Molecular Weight:400.634
Hs Code.:

Synonyms:2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl tert-butyldimethylsilylether

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Chemical Property of 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl tert-butyldimethylsilylether

Chemical Property:

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Technology Process of 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl tert-butyldimethylsilylether

There total 3 articles about 2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl tert-butyldimethylsilylether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 3587-60-8
Benzyloxymethyl chloride

: 174867-46-0
2-(1-hydroxy-1-methylethyl)-4-methylphenyl tert-butyldimethylsilylether

: 174867-47-1
2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl tert-butyldimethylsilylether

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 72h;

Reference yield:

: 6627-55-0
2-bromo-p-cresol

: 174867-47-1
2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl tert-butyldimethylsilylether

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / n-BuLi / hexane; diethyl ether / 1.) room temperature, 2 h, 2.) -78 deg C -> 0 deg C, 1 h

2: 70 percent / N,N-diisopropylethylamine / dimethylformamide

3: 80 percent / N,N-diisopropylethylamine / tetrahydrofuran / 72 h

With n-butyllithium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; N,N-dimethyl-formamide;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 174867-47-1
2-<1-(benzyloxymethoxy)-1-methylethyl>-4-methylphenyl tert-butyldimethylsilylether

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / N,N-diisopropylethylamine / dimethylformamide

2: 80 percent / N,N-diisopropylethylamine / tetrahydrofuran / 72 h

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;