o-Diethylphosphinylmethylphenol

Base Information

Chemical Name:o-Diethylphosphinylmethylphenol
CAS No.:70127-51-4
Molecular Formula:C₁₁H₁₇O₂P
Molecular Weight:212.229
Hs Code.:
DSSTox Substance ID:DTXSID501294449

Synonyms:o-diethylphosphinylmethylphenol;SCHEMBL10910024;DTXSID501294449;2-[(Diethylphosphinyl)methyl]phenol;70127-51-4

Suppliers and Price of o-Diethylphosphinylmethylphenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of o-Diethylphosphinylmethylphenol

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:212.09661678
Heavy Atom Count:14
Complexity:207

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCP(=O)(CC)CC1=CC=CC=C1O

Technology Process of o-Diethylphosphinylmethylphenol

There total 3 articles about o-Diethylphosphinylmethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 70127-51-4
diethyl(2-hydroxybenzyl)phosphine oxide

Guidance literature:

Reference yield: 54.0%

: 74-96-4
ethyl bromide

: 14707-41-6
2-ethoxy-2,3-dihydro-[d][1,2]oxaphosphole 2-oxide

: 70127-51-4
diethyl(2-hydroxybenzyl)phosphine oxide

Guidance literature:: ethyl bromide; With magnesium; In tetrahydrofuran;

2-ethoxy-2,3-dihydro-[d][1,2]oxaphosphole 2-oxide; In tetrahydrofuran; for 2h; Reflux; Inert atmosphere;

With sulfuric acid; In tetrahydrofuran; water;
DOI:10.1134/S1070363216030063

Reference yield:

: 90-01-7
salicylic alcohol

: 70127-51-4
diethyl(2-hydroxybenzyl)phosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 12 h / Reflux

2.1: magnesium / tetrahydrofuran

2.2: 2 h / Reflux; Inert atmosphere

With magnesium; In tetrahydrofuran; toluene;
DOI:10.1134/S1070363216030063