1-bromo-3-phenylselenopropane

Base Information

Chemical Name:1-bromo-3-phenylselenopropane
CAS No.:118824-31-0
Molecular Formula:C₉H₁₁BrSe
Molecular Weight:278.05
Hs Code.:

Synonyms:1-bromo-3-phenylselenopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-bromo-3-phenylselenopropane

Chemical Property:

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Technology Process of 1-bromo-3-phenylselenopropane

There total 3 articles about 1-bromo-3-phenylselenopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1666-13-3
diphenyl diselenide

: 109-64-8
1,3-dibromo-propane

: 118824-31-0
1-bromo-3-phenylselenopropane

Guidance literature:: diphenyl diselenide; With sodium tetrahydroborate; In ethanol; at 0 ℃; Inert atmosphere;

1,3-dibromo-propane; In ethanol; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201808605

Reference yield: 61.0%

: 70813-85-3
γ-Phenylselenenylpropanol

: 118824-31-0
1-bromo-3-phenylselenopropane

Guidance literature:: With N-Bromosuccinimide; triphenylphosphine; In acetonitrile; at 0 ℃; for 3h;
DOI:10.1016/S0040-4020(01)85436-3

Reference yield:

: 1666-13-3
diphenyl diselenide

: 118824-31-0
1-bromo-3-phenylselenopropane

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Na / 1) THF, room temperature, 5 h, ultrasound, 2) room temperature

2: 61 percent / NBS, Ph₃P / acetonitrile / 3 h / 0 °C

With N-Bromosuccinimide; sodium; triphenylphosphine; In acetonitrile;
DOI:10.1016/S0040-4020(01)85436-3