1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-(2-hydroxyethyl)-3,6-dihydro-1(2H)-pyridinecarboxylate

Base Information

Chemical Name:1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-(2-hydroxyethyl)-3,6-dihydro-1(2H)-pyridinecarboxylate
CAS No.:1013097-77-2
Molecular Formula:C₁₈H₂₃Cl₂NO₃
Molecular Weight:372.292
Hs Code.:

Synonyms:1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-(2-hydroxyethyl)-3,6-dihydro-1(2H)-pyridinecarboxylate

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Chemical Property of 1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-(2-hydroxyethyl)-3,6-dihydro-1(2H)-pyridinecarboxylate

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Technology Process of 1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-(2-hydroxyethyl)-3,6-dihydro-1(2H)-pyridinecarboxylate

There total 1 articles about 1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-(2-hydroxyethyl)-3,6-dihydro-1(2H)-pyridinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1013097-76-1
1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-[2-(ethyloxy)-2-oxoethyl]-3,6-dihydro-1(2H)-pyridinecarboxylate

: 3-(1,1-dimethylethyl) 7-ethyl (1S,6R/1R,6S)-6-(3,4-dichlorophenyl)-3-azabicyclo[4.1.0]heptane-3,7-dicarboxylate

: 1013097-77-2
1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-(2-hydroxyethyl)-3,6-dihydro-1(2H)-pyridinecarboxylate

: 1,1-dimethylethyl (1S,6R/1R,6S)-6-(3,4-dichlorophenyl)-7-hydroxymethyl-3-azabicyclo[4.1.0]heptane-3-carboxylate

Guidance literature:: 1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-[2-(ethyloxy)-2-oxoethyl]-3,6-dihydro-1(2H)-pyridinecarboxylate; 3-(1,1-dimethylethyl) 7-ethyl (1S,6R/1R,6S)-6-(3,4-dichlorophenyl)-3-azabicyclo[4.1.0]heptane-3,7-dicarboxylate; With lithium aluminium tetrahydride; In diethyl ether; toluene; at -20 ℃; for 1h;

With water; ammonium chloride; In diethyl ether; toluene;

Reference yield:

: 1013097-77-2
1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-(2-hydroxyethyl)-3,6-dihydro-1(2H)-pyridinecarboxylate

: 74-88-4
methyl iodide

: 1013097-78-3
1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-(2-methoxyethyl)-3,6-dihydro-1(2H)-pyridinecarboxylate

: 1,1-dimethylethyl (1S,6R/1R,6S)-6-(3,4-dichlorophenyl)-7-methoxymethyl-3-azabicyclo[4.1.0]heptane-3-carboxylate

Guidance literature:: 1,1-dimethylethyl 4-(3,4-dichlorophenyl)-6-(2-hydroxyethyl)-3,6-dihydro-1(2H)-pyridinecarboxylate; 1,1-dimethylethyl (1S,6R/1R,6S)-6-(3,4-dichlorophenyl)-7-hydroxymethyl-3-azabicyclo[4.1.0]heptane-3-carboxylate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;