4-(1-(4-(dimethylamino)phenyl)-2-(thiophen-2-yl)vinyl)-N,N-dimethylbenzenamine

Base Information

Chemical Name:4-(1-(4-(dimethylamino)phenyl)-2-(thiophen-2-yl)vinyl)-N,N-dimethylbenzenamine
CAS No.:1008756-41-9
Molecular Formula:C₂₂H₂₄N₂S
Molecular Weight:348.512
Hs Code.:

Synonyms:4-(1-(4-(dimethylamino)phenyl)-2-(thiophen-2-yl)vinyl)-N,N-dimethylbenzenamine

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Chemical Property of 4-(1-(4-(dimethylamino)phenyl)-2-(thiophen-2-yl)vinyl)-N,N-dimethylbenzenamine

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Technology Process of 4-(1-(4-(dimethylamino)phenyl)-2-(thiophen-2-yl)vinyl)-N,N-dimethylbenzenamine

There total 2 articles about 4-(1-(4-(dimethylamino)phenyl)-2-(thiophen-2-yl)vinyl)-N,N-dimethylbenzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 77295-66-0
2-(2,2-dibromovinyl)thiophene

: 171364-78-6
(4-(N,N-dimethylamino)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1008756-41-9
4-(1-(4-(dimethylamino)phenyl)-2-(thiophen-2-yl)vinyl)-N,N-dimethylbenzenamine

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; for 45h; Heating;
DOI:10.1016/j.tetlet.2007.12.010

Reference yield: 44.0%

: 98-03-3
thiophene-2-carbaldehyde

: diethyl bis[4-(dimethylamino)phenyl]methylphosphonate

: 1008756-41-9
4-(1-(4-(dimethylamino)phenyl)-2-(thiophen-2-yl)vinyl)-N,N-dimethylbenzenamine

Guidance literature:: diethyl bis[4-(dimethylamino)phenyl]methylphosphonate; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

thiophene-2-carbaldehyde; In tetrahydrofuran; at 0 - 20 ℃; for 13h; Inert atmosphere;
DOI:10.1002/cjoc.201190066