1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranose

Base Information

Chemical Name:1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranose
CAS No.:470667-86-8
Molecular Formula:C₃₃H₄₀O₁₉
Molecular Weight:740.669
Hs Code.:

Synonyms:1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranose

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Chemical Property of 1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranose

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Technology Process of 1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranose

There total 4 articles about 1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 470667-86-8
1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-iodosuccinimide; trifluoromethanesulfonic acid; 4 Angstroem molecular sieves / CH₂Cl₂; diethyl ether / 0.33 h / -30 °C

1.2: 40 percent / pyridine / 2.33 h / 80 °C

2.1: H₂; AcOH / Pd/C / 32 h / 20 °C / 1725.14 Torr

3.1: 1.39 g / pyridine / 19 h / 20 °C

4.1: BF₃*Et₂O / toluene / 1 h / 20 °C

With pyridine; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; boron trifluoride diethyl etherate; hydrogen; acetic acid; palladium on activated charcoal; In diethyl ether; dichloromethane; toluene;
DOI:10.1081/car-120004332

Reference yield:

: 2-(trimethylsilyl)ethyl 2-O-benzoyl-4,6-di-O-benzylidene-3-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-β-D-galactopyranoside

: 470667-86-8
1,4,6-tri-O-acetyl-2-O-benzoyl-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: H₂; AcOH / Pd/C / 32 h / 20 °C / 1725.14 Torr

2: 1.39 g / pyridine / 19 h / 20 °C

3: BF₃*Et₂O / toluene / 1 h / 20 °C

With pyridine; boron trifluoride diethyl etherate; hydrogen; acetic acid; palladium on activated charcoal; In toluene;
DOI:10.1081/car-120004332