methyl 4,6-O-benzylidene-2-deoxy-2-phenylthio-α-D-lyxo-hexopyranosid-3-ulose phenylhydrazone

Base Information

Chemical Name:methyl 4,6-O-benzylidene-2-deoxy-2-phenylthio-α-D-lyxo-hexopyranosid-3-ulose phenylhydrazone
CAS No.:86030-27-5
Molecular Formula:C₂₆H₂₆N₂O₄S
Molecular Weight:462.569
Hs Code.:

Synonyms:methyl 4,6-O-benzylidene-2-deoxy-2-phenylthio-α-D-lyxo-hexopyranosid-3-ulose phenylhydrazone

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Chemical Property of methyl 4,6-O-benzylidene-2-deoxy-2-phenylthio-α-D-lyxo-hexopyranosid-3-ulose phenylhydrazone

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Technology Process of methyl 4,6-O-benzylidene-2-deoxy-2-phenylthio-α-D-lyxo-hexopyranosid-3-ulose phenylhydrazone

There total 5 articles about methyl 4,6-O-benzylidene-2-deoxy-2-phenylthio-α-D-lyxo-hexopyranosid-3-ulose phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 108-98-5
thiophenol

: 86030-23-1
methyl 4,6-O-benzylidene-2,3-dideoxy-3-phenylazo-α-D-threo-hex-2-enopyranoside

: 86030-27-5
methyl 4,6-O-benzylidene-2-deoxy-2-phenylthio-α-D-lyxo-hexopyranosid-3-ulose phenylhydrazone

Guidance literature:: With sodium hydride; In acetone; at 40 - 45 ℃; for 0.166667h;

Reference yield:

: 64552-06-3
methyl 4,6-O-benzylidene-α-D-galactopyranoside

: 86030-27-5
methyl 4,6-O-benzylidene-2-deoxy-2-phenylthio-α-D-lyxo-hexopyranosid-3-ulose phenylhydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: 21 percent / triethylamine / acetonitrile / 0.25 h

2: 75 percent / DMSO, dicyclohexylcarbodi-imide, anhydrous phosphoric acid / 24 h / Ambient temperature

3: 85 percent / glacial acetic acid / dimethylformamide / 20 h / Ambient temperature

4: 73 percent / sodium hydride / acetone / 0.17 h / 40 - 45 °C

With phosphoric acid; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 28642-65-1,38993-04-3,68366-59-6,75879-92-4,109010-31-3,109010-34-6
methyl 2-O-benzoyl-4,6-O-benzylidene-α-D-xylo-hexopyranosid-3-ulose

: 86030-27-5
methyl 4,6-O-benzylidene-2-deoxy-2-phenylthio-α-D-lyxo-hexopyranosid-3-ulose phenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / glacial acetic acid / dimethylformamide / 20 h / Ambient temperature

2: 73 percent / sodium hydride / acetone / 0.17 h / 40 - 45 °C

With sodium hydride; acetic acid; In N,N-dimethyl-formamide; acetone;