2-(2-chloro-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-o-tolylacetamide

Base Information

Chemical Name:2-(2-chloro-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-o-tolylacetamide
CAS No.:1260403-17-5
Molecular Formula:C₁₈H₁₃Br₂ClN₂OS₂
Molecular Weight:532.707
Hs Code.:

Synonyms:2-(2-chloro-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-o-tolylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-chloro-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-o-tolylacetamide

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Technology Process of 2-(2-chloro-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-o-tolylacetamide

There total 6 articles about 2-(2-chloro-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-o-tolylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.6%

: 1260403-09-5
2-(2-amino-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-o-tolylacetamide

: 1260403-17-5
2-(2-chloro-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-o-tolylacetamide

Guidance literature:: With tert.-butylnitrite; copper(l) chloride; In acetonitrile; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1007/s12272-012-0604-y

Reference yield:

: 1385770-66-0
C₁₂H₁₁Br₃O₃S

: 1260403-17-5
2-(2-chloro-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-o-tolylacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: ethanol / 20 °C

2: sodium hydroxide / dimethyl sulfoxide / 4 h / 20 °C

3: phosphorus pentachloride / diethyl ether / 5 h / 20 °C

4: triethylamine / dichloromethane / 10 h / 20 °C / Cooling with ice

5: tert.-butylnitrite; copper(l) chloride / acetonitrile / 0.25 h / 20 °C / Inert atmosphere

With tert.-butylnitrite; phosphorus pentachloride; triethylamine; copper(l) chloride; sodium hydroxide; In diethyl ether; ethanol; dichloromethane; dimethyl sulfoxide; acetonitrile; 5: Sandmeyer reaction;
DOI:10.1007/s12272-012-0604-y

Reference yield:

: 108-36-1
1,3-dibromobenzene

: 1260403-17-5
2-(2-chloro-4-(2,4-dibromophenyl)thiazol-5-ylthio)-N-o-tolylacetamide

Guidance literature:: Multi-step reaction with 8 steps

1: aluminum (III) chloride / 20 - 65 °C

2: sodium carbonate / ethanol / 12 h / 20 °C

3: bromine / acetic acid / 8.5 h / 20 °C

4: ethanol / 20 °C

5: sodium hydroxide / dimethyl sulfoxide / 4 h / 20 °C

6: phosphorus pentachloride / diethyl ether / 5 h / 20 °C

7: triethylamine / dichloromethane / 10 h / 20 °C / Cooling with ice

8: tert.-butylnitrite; copper(l) chloride / acetonitrile / 0.25 h / 20 °C / Inert atmosphere

With aluminum (III) chloride; tert.-butylnitrite; phosphorus pentachloride; bromine; sodium carbonate; triethylamine; copper(l) chloride; sodium hydroxide; In diethyl ether; ethanol; dichloromethane; acetic acid; dimethyl sulfoxide; acetonitrile; 1: Friedel Crafts reaction / 8: Sandmeyer reaction;
DOI:10.1007/s12272-012-0604-y