Biphenyl-4-carboxylic acid (2R,3R,5R)-3-acetoxy-3-(tert-butyl-dimethyl-silanyloxymethyl)-5-methoxy-tetrahydro-furan-2-ylmethyl ester

Base Information

Chemical Name:Biphenyl-4-carboxylic acid (2R,3R,5R)-3-acetoxy-3-(tert-butyl-dimethyl-silanyloxymethyl)-5-methoxy-tetrahydro-furan-2-ylmethyl ester
CAS No.:199177-92-9
Molecular Formula:C₂₈H₃₈O₇Si
Molecular Weight:514.691
Hs Code.:

Synonyms:Biphenyl-4-carboxylic acid (2R,3R,5R)-3-acetoxy-3-(tert-butyl-dimethyl-silanyloxymethyl)-5-methoxy-tetrahydro-furan-2-ylmethyl ester

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Chemical Property of Biphenyl-4-carboxylic acid (2R,3R,5R)-3-acetoxy-3-(tert-butyl-dimethyl-silanyloxymethyl)-5-methoxy-tetrahydro-furan-2-ylmethyl ester

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Technology Process of Biphenyl-4-carboxylic acid (2R,3R,5R)-3-acetoxy-3-(tert-butyl-dimethyl-silanyloxymethyl)-5-methoxy-tetrahydro-furan-2-ylmethyl ester

There total 3 articles about Biphenyl-4-carboxylic acid (2R,3R,5R)-3-acetoxy-3-(tert-butyl-dimethyl-silanyloxymethyl)-5-methoxy-tetrahydro-furan-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 108-24-7
acetic anhydride

: 199177-91-8
Biphenyl-4-carboxylic acid (2R,3R,5R)-3-(tert-butyl-dimethyl-silanyloxymethyl)-3-hydroxy-5-methoxy-tetrahydro-furan-2-ylmethyl ester

: 199177-92-9
Biphenyl-4-carboxylic acid (2R,3R,5R)-3-acetoxy-3-(tert-butyl-dimethyl-silanyloxymethyl)-5-methoxy-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: With dmap; In pyridine; dichloromethane;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 199177-92-9
Biphenyl-4-carboxylic acid (2R,3R,5R)-3-acetoxy-3-(tert-butyl-dimethyl-silanyloxymethyl)-5-methoxy-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / imidazole / dimethylformamide / 3.5 h / Ambient temperature

2: 94 percent / DMAP, pyridine / CH₂Cl₂ / 24 h / Ambient temperature

With pyridine; 1H-imidazole; dmap; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 172293-93-5
Biphenyl-4-carboxylic acid (2R,3R,5R)-3-hydroxy-3-hydroxymethyl-5-methoxy-tetrahydro-furan-2-ylmethyl ester

: 199177-92-9
Biphenyl-4-carboxylic acid (2R,3R,5R)-3-acetoxy-3-(tert-butyl-dimethyl-silanyloxymethyl)-5-methoxy-tetrahydro-furan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / imidazole / dimethylformamide / 3.5 h / Ambient temperature

2: 94 percent / DMAP, pyridine / CH₂Cl₂ / 24 h / Ambient temperature

With pyridine; 1H-imidazole; dmap; In dichloromethane; N,N-dimethyl-formamide;