(E)-N-[4-(1-{[diaminomethylene]hydrazono}ethyl)phenyl]-4-nitrobenzamide hydrochloride

Base Information

Chemical Name:(E)-N-[4-(1-{[diaminomethylene]hydrazono}ethyl)phenyl]-4-nitrobenzamide hydrochloride
CAS No.:1020087-09-5
Molecular Formula:C₁₆H₁₆N₆O₃*ClH
Molecular Weight:376.802
Hs Code.:

Synonyms:(E)-N-[4-(1-{[diaminomethylene]hydrazono}ethyl)phenyl]-4-nitrobenzamide hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-[4-(1-{[diaminomethylene]hydrazono}ethyl)phenyl]-4-nitrobenzamide hydrochloride

Chemical Property:

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Technology Process of (E)-N-[4-(1-{[diaminomethylene]hydrazono}ethyl)phenyl]-4-nitrobenzamide hydrochloride

There total 4 articles about (E)-N-[4-(1-{[diaminomethylene]hydrazono}ethyl)phenyl]-4-nitrobenzamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: (E)-N-[4-(1-{diaminomethylene}hydrazono)ethyl]-4-benzamine dihydrochloride

: 122-04-3
4-nitro-benzoyl chloride

: 1020087-09-5
(E)-N-[4-(1-{[diaminomethylene]hydrazono}ethyl)phenyl]-4-nitrobenzamide hydrochloride

Guidance literature:: With pyridine; In 1,4-dioxane; for 2h; Heating / reflux;

Reference yield: 29.0%

: (E)-N-[4-(1-{diaminomethylene}hydrazono)ethyl]-4-benzamine dihydrochloride

: 122-04-3
4-nitro-benzoyl chloride

: 1020087-09-5
(E)-N-[4-(1-{[diaminomethylene]hydrazono}ethyl)phenyl]-4-nitrobenzamide hydrochloride

Guidance literature:: With pyridine; In 1,4-dioxane; for 2h; Reflux;
DOI:10.1016/j.bmc.2013.03.033

Reference yield:

: 100-19-6
(4-nitrophenyl)ethanone

: 1020087-09-5
(E)-N-[4-(1-{[diaminomethylene]hydrazono}ethyl)phenyl]-4-nitrobenzamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / methanol; water / 1 h / Reflux

2: iron; hydrogenchloride / water; ethanol / 14 h / Reflux

3: pyridine / 1,4-dioxane / 2 h / Reflux

With pyridine; hydrogenchloride; iron; In 1,4-dioxane; methanol; ethanol; water;
DOI:10.1016/j.bmc.2013.03.033