((1R,2S,5R,6R)-8-Bromo-3,4-diaza-tricyclo[4.2.1.0^2,5]non-3-en-7-yl)-(4-chloro-phenyl)-amine

Base Information

• Chemical Name: ((1R,2S,5R,6R)-8-Bromo-3,4-diaza-tricyclo[4.2.1.0^2,5]non-3-en-7-yl)-(4-chloro-phenyl)-amine
• CAS No.: 70417-49-1
• Molecular Formula: C₁₃H₁₃BrClN₃
• Molecular Weight: 326.623

Synonyms:((1R,2S,5R,6R)-8-Bromo-3,4-diaza-tricyclo[4.2.1.0^2,5]non-3-en-7-yl)-(4-chloro-phenyl)-amine

Chemical Property of ((1R,2S,5R,6R)-8-Bromo-3,4-diaza-tricyclo[4.2.1.0^2,5]non-3-en-7-yl)-(4-chloro-phenyl)-amine

Chemical Property:

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Technology Process of ((1R,2S,5R,6R)-8-Bromo-3,4-diaza-tricyclo[4.2.1.0^2,5]non-3-en-7-yl)-(4-chloro-phenyl)-amine

There total 4 articles about ((1R,2S,5R,6R)-8-Bromo-3,4-diaza-tricyclo[4.2.1.0^2,5]non-3-en-7-yl)-(4-chloro-phenyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C13H12ClN5 (65245-23-0,77788-21-7) → ((1R,2S,5R,6R)-8-Bromo-3,4-diaza-tricyclo[4.2.1.02,5]non-3-en-7-yl)-(4-chloro-phenyl)-amine (70417-49-1)

Guidance literature:

With hydrogen bromide; at 100 ℃; for 3h;

Reference yield:

1-azido-4-chlorobenzene (3296-05-7) → ((1R,2S,5R,6R)-8-Bromo-3,4-diaza-tricyclo[4.2.1.02,5]non-3-en-7-yl)-(4-chloro-phenyl)-amine (70417-49-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / toluene / 12 h / 80 °C

2: 86 percent / 7.5percent aq. HBr / 3 h / 100 °C

With hydrogen bromide; In toluene;

Reference yield:

exo-3,4-diazotricyclo[4.2.1.02,5]nona-3,7-diene (23979-29-5) → ((1R,2S,5R,6R)-8-Bromo-3,4-diaza-tricyclo[4.2.1.02,5]non-3-en-7-yl)-(4-chloro-phenyl)-amine (70417-49-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / toluene / 12 h / 80 °C

2: 86 percent / 7.5percent aq. HBr / 3 h / 100 °C

With hydrogen bromide; In toluene;

upstream raw materials:

C₁₃H₁₂ClN₅

1-azido-4-chlorobenzene

exo-3,4-diazotricyclo[4.2.1.0^2,5]nona-3,7-diene

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