Technology Process of C12H16ClNO3*ClH
There total 4 articles about C12H16ClNO3*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; water;
In
1,4-dioxane;
at 50 ℃;
for 6h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl acetamide / 16 h / 60 °C
2: thiophene; hydrogen / platinum on activated charcoal; vanadia / di-isopropyl ether; ethyl acetate / 20 h / 20 °C
3: hydrogenchloride; water / 1,4-dioxane / 6 h / 50 °C
With
thiophene; hydrogenchloride; water; hydrogen; potassium carbonate;
platinum on activated charcoal; vanadia;
In
1,4-dioxane; di-isopropyl ether; N,N-dimethyl acetamide; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: thiophene; hydrogen / platinum on activated charcoal; vanadia / di-isopropyl ether; ethyl acetate / 20 h / 20 °C
2: hydrogenchloride; water / 1,4-dioxane / 6 h / 50 °C
With
thiophene; hydrogenchloride; water; hydrogen;
platinum on activated charcoal; vanadia;
In
1,4-dioxane; di-isopropyl ether; ethyl acetate;