(Z)-1,1-Dimethylethyl 3-amino-3-<7'-(3,4-dimethoxyphenyl)bicyclo<4.2.0>octa-1',3',5'-trien-7'-yl>propenoate

Base Information

Chemical Name:(Z)-1,1-Dimethylethyl 3-amino-3-<7'-(3,4-dimethoxyphenyl)bicyclo<4.2.0>octa-1',3',5'-trien-7'-yl>propenoate
CAS No.:142532-27-2
Molecular Formula:C₂₃H₂₇NO₄
Molecular Weight:381.472
Hs Code.:

Synonyms:(Z)-1,1-Dimethylethyl 3-amino-3-<7'-(3,4-dimethoxyphenyl)bicyclo<4.2.0>octa-1',3',5'-trien-7'-yl>propenoate

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Chemical Property of (Z)-1,1-Dimethylethyl 3-amino-3-<7'-(3,4-dimethoxyphenyl)bicyclo<4.2.0>octa-1',3',5'-trien-7'-yl>propenoate

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Technology Process of (Z)-1,1-Dimethylethyl 3-amino-3-<7'-(3,4-dimethoxyphenyl)bicyclo<4.2.0>octa-1',3',5'-trien-7'-yl>propenoate

There total 5 articles about (Z)-1,1-Dimethylethyl 3-amino-3-<7'-(3,4-dimethoxyphenyl)bicyclo<4.2.0>octa-1',3',5'-trien-7'-yl>propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 540-88-5
acetic acid tert-butyl ester

: 142532-22-7
7-(3,4-Dimethoxyphenyl)bicyclo<4.2.0>octa-1,3,5-triene-7-carbonitrile

: 142532-27-2
(Z)-1,1-Dimethylethyl 3-amino-3-<7'-(3,4-dimethoxyphenyl)bicyclo<4.2.0>octa-1',3',5'-trien-7'-yl>propenoate

Guidance literature:: With magnesium bis(N,N-diisopropylamide); In tetrahydrofuran; diethyl ether; at 0 ℃; for 1.5h;

Reference yield:

: 3469-06-5
benzocyclobutenone

: 142532-27-2
(Z)-1,1-Dimethylethyl 3-amino-3-<7'-(3,4-dimethoxyphenyl)bicyclo<4.2.0>octa-1',3',5'-trien-7'-yl>propenoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg / 1.) THF, 2.) -40 deg C, 30 min

2: 57 percent / zinc iodide / CH₂Cl₂ / 25 h / 0 °C

3: 69 percent / magnesium bis(diisopropylamide) / diethyl ether; tetrahydrofuran / 1.5 h / 0 °C

With magnesium; magnesium bis(N,N-diisopropylamide); zinc(II) iodide; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 142532-19-2
7-(3,4-Dimethoxyphenyl)bicyclo<4.2.0>octa-1,3,5-trien-7-ol

: 142532-27-2
(Z)-1,1-Dimethylethyl 3-amino-3-<7'-(3,4-dimethoxyphenyl)bicyclo<4.2.0>octa-1',3',5'-trien-7'-yl>propenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / zinc iodide / CH₂Cl₂ / 25 h / 0 °C

2: 69 percent / magnesium bis(diisopropylamide) / diethyl ether; tetrahydrofuran / 1.5 h / 0 °C

With magnesium bis(N,N-diisopropylamide); zinc(II) iodide; In tetrahydrofuran; diethyl ether; dichloromethane;