C₁₅H₁₅⁽²⁾HN₂O₂

Base Information

Chemical Name:C₁₅H₁₅⁽²⁾HN₂O₂
CAS No.:1620194-11-7
Molecular Formula:C₁₅H₁₆N₂O₂
Molecular Weight:257.296
Hs Code.:

C<sub>15</sub>H<sub>15</sub><sup>(2)</sup>HN<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₅H₁₅⁽²⁾HN₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₁₅⁽²⁾HN₂O₂

Chemical Property:

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Technology Process of C₁₅H₁₅⁽²⁾HN₂O₂

There total 4 articles about C₁₅H₁₅⁽²⁾HN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620194-08-2
N-(2-(pyridin-2-yl)propan-2-yl)benzamide-2-d₁

: N-(2-(pyridin-2-yl)propan-2-yl)benzamide

: 1620194-11-7
C₁₅H₁₅⁽²⁾HN₂O₂

Guidance literature:: With copper diacetate; tetra-(n-butyl)ammonium iodide; silver carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 0.266667h; Overall yield = 45 %; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol5016064

Reference yield:

: 22069-99-4
1-bromo-2-deuterobenzene

: 1620194-11-7
C₁₅H₁₅⁽²⁾HN₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran / 0.67 h / -78 °C

1.2: 0.33 h / -78 °C

2.1: thionyl chloride / 2 h / Reflux

3.1: triethylamine / dichloromethane / 6 h / 0 - 20 °C

4.1: copper diacetate; silver carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 0.27 h / 100 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; thionyl chloride; copper diacetate; tetra-(n-butyl)ammonium iodide; triethylamine; silver carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol5016064

Reference yield:

: 583-55-1
1-Bromo-2-iodobenzene

: 1620194-11-7
C₁₅H₁₅⁽²⁾HN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran; diethyl ether / 2 h / -78 °C

1.2: 0.5 h / -78 - 20 °C

2.1: n-butyllithium / tetrahydrofuran / 0.67 h / -78 °C

2.2: 0.33 h / -78 °C

3.1: thionyl chloride / 2 h / Reflux

4.1: triethylamine / dichloromethane / 6 h / 0 - 20 °C

5.1: copper diacetate; silver carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 0.27 h / 100 °C / Inert atmosphere; Schlenk technique

With n-butyllithium; thionyl chloride; isopropylmagnesium chloride; copper diacetate; tetra-(n-butyl)ammonium iodide; triethylamine; silver carbonate; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol5016064