D-glycero-2,3-dihydroxy-2,3-O-isopropylidenepropyl 4-O-benzyl-2,3-di-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyrnaoside

Base Information

Chemical Name:D-glycero-2,3-dihydroxy-2,3-O-isopropylidenepropyl 4-O-benzyl-2,3-di-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyrnaoside
CAS No.:399511-08-1
Molecular Formula:C₂₆H₄₀O₈
Molecular Weight:480.599
Hs Code.:

Synonyms:D-glycero-2,3-dihydroxy-2,3-O-isopropylidenepropyl 4-O-benzyl-2,3-di-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyrnaoside

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Chemical Property of D-glycero-2,3-dihydroxy-2,3-O-isopropylidenepropyl 4-O-benzyl-2,3-di-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyrnaoside

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Technology Process of D-glycero-2,3-dihydroxy-2,3-O-isopropylidenepropyl 4-O-benzyl-2,3-di-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyrnaoside

There total 1 articles about D-glycero-2,3-dihydroxy-2,3-O-isopropylidenepropyl 4-O-benzyl-2,3-di-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyrnaoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 23788-74-1,7305-59-1
(R)-2,2-dimethyl-1,3-dioxolane-4-ylmethyl p-toluenesulfonate

: 399510-98-6
4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranose

: 399511-08-1
D-glycero-2,3-dihydroxy-2,3-O-isopropylidenepropyl 4-O-benzyl-2,3-di-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyrnaoside

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 90 ℃; for 8h;
DOI:10.1002/1099-0690(200111)2001:21<4127::AID-EJOC4127>3.0.CO;2-6

Reference yield: 69.0%

: 399511-08-1
D-glycero-2,3-dihydroxy-2,3-O-isopropylidenepropyl 4-O-benzyl-2,3-di-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyrnaoside

: 331980-98-4
D-glycero-2,3-dihydroxypropyl 4-O-benzyl-5a-carba-α-L-fucopyranoside

Guidance literature:: With water; acetic acid; at 100 ℃; for 2h;
DOI:10.1002/1099-0690(200111)2001:21<4127::AID-EJOC4127>3.0.CO;2-6

Reference yield:

: 399511-08-1
D-glycero-2,3-dihydroxy-2,3-O-isopropylidenepropyl 4-O-benzyl-2,3-di-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyrnaoside

: D-glycero-2,3-dihydroxypropyl 5a-carba-α-L-fucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / AcOH; water / 2 h / 100 °C

2: 76 percent / H₂ / Pd/C / methanol / 2 h / 20 °C

With water; hydrogen; acetic acid; palladium on activated charcoal; In methanol;
DOI:10.1002/1099-0690(200111)2001:21<4127::AID-EJOC4127>3.0.CO;2-6