4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranose

Base Information

Chemical Name:4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranose
CAS No.:399510-98-6
Molecular Formula:C₂₀H₃₀O₆
Molecular Weight:366.455
Hs Code.:

Synonyms:4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranose

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Chemical Property of 4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranose

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Technology Process of 4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranose

There total 1 articles about 4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 431-03-8
dimethylglyoxal

: 399510-94-2
4-O-benzyl-5a-carba-α-L-fucopyranose

: 149-73-5
trimethyl orthoformate

: 399510-98-6
4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranose

Guidance literature:: With camphor-10-sulfonic acid; In methanol; at 60 ℃; for 12h;
DOI:10.1002/1099-0690(200111)2001:21<4127::AID-EJOC4127>3.0.CO;2-6

Reference yield: 96.0%

: 399510-98-6
4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranose

: 74-88-4
methyl iodide

: 399511-03-6
methyl 4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranoside

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1002/1099-0690(200111)2001:21<4127::AID-EJOC4127>3.0.CO;2-6

Reference yield: 73.0%

: 23735-43-5,7305-59-1
(S)-1-O-tosyl-2,3-O-isopropylideneglycerol

: 399510-98-6
4-O-benzyl-2,3-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyranose

: 399511-15-0
L-glycero-2,3-dihydroxy-2,3-O-isopropylidenepropyl 4-O-benzyl-2,3-di-O-(2,3-dimethoxybutane-2,3-diyl)-5a-carba-α-L-fucopyrnaoside

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 90 ℃; for 8h;
DOI:10.1002/1099-0690(200111)2001:21<4127::AID-EJOC4127>3.0.CO;2-6