C₁₃H₂₂⁽²⁾HNO

Base Information

Chemical Name:C₁₃H₂₂⁽²⁾HNO
CAS No.:80997-38-2
Molecular Formula:C₁₃H₂₃NO
Molecular Weight:210.324
Hs Code.:

C<sub>13</sub>H<sub>22</sub><sup>(2)</sup>HNO

Synonyms:C₁₃H₂₂⁽²⁾HNO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₂₂⁽²⁾HNO

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Technology Process of C₁₃H₂₂⁽²⁾HNO

There total 3 articles about C₁₃H₂₂⁽²⁾HNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 80997-37-1
N,N-diisopropyl-1-cyclohexenecarboxamide

: 80997-38-2
C₁₃H₂₂⁽²⁾HNO

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; water-d2; sec.-butyllithium; In tetrahydrofuran; 1.) -78 deg C; 2.) -78 deg C to RT;
DOI:10.1021/ja00302a024

Reference yield:

: 636-82-8
cyclohexene-1-carboxylic acid

: 80997-38-2
C₁₃H₂₂⁽²⁾HNO

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 2.5 h / Heating

2: diethyl ether / 4 h / Ambient temperature

3: 85 percent / deuterium oxide, sec-BuLi, TMEDA / tetrahydrofuran / 1.) -78 deg C; 2.) -78 deg C to RT

With thionyl chloride; N,N,N,N,-tetramethylethylenediamine; water-d2; sec.-butyllithium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00302a024

Reference yield:

: 36278-22-5
1-cyclohexenoyl chloride

: 80997-38-2
C₁₃H₂₂⁽²⁾HNO

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 4 h / Ambient temperature

2: 85 percent / deuterium oxide, sec-BuLi, TMEDA / tetrahydrofuran / 1.) -78 deg C; 2.) -78 deg C to RT

With N,N,N,N,-tetramethylethylenediamine; water-d2; sec.-butyllithium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00302a024