C₂₂H₂₉NO₇

Base Information

Chemical Name:C₂₂H₂₉NO₇
CAS No.:850359-86-3
Molecular Formula:C₂₂H₂₉NO₇
Molecular Weight:419.475
Hs Code.:

C<sub>22</sub>H<sub>29</sub>NO<sub>7</sub>

Synonyms:C₂₂H₂₉NO₇

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Chemical Property of C₂₂H₂₉NO₇

Chemical Property:

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Technology Process of C₂₂H₂₉NO₇

There total 11 articles about C₂₂H₂₉NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 100-39-0
benzyl bromide

: 850359-69-2
C₁₅H₂₃NO₇

: 850359-86-3
C₂₂H₂₉NO₇

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1055/s-2004-837223

Reference yield:

: 2847-00-9
1,2:5,6-di-O-isopropylidene-α-D-hexofuran-3-ulose

: 850359-86-3
C₂₂H₂₉NO₇

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene / 100 °C

2.1: 99 percent / DIBALH / CH₂Cl₂ / -20 °C

3.1: DBU / CH₂Cl₂ / -78 °C

4.1: K₂CO₃ / xylene / Heating

5.1: O₃ / CH₂Cl₂ / -78 °C

5.2: 90 percent / Et₃N / CH₂Cl₂ / 0 °C

6.1: 95 percent / tetrahydrofuran / 0 °C

7.1: 96 percent / DMSO; Ac₂O / 20 °C

8.1: 70 percent / NaBH₄; CeCl₃*7H₂O / CH₂Cl₂; methanol / -10 °C

9.1: 99 percent / DBU / CH₂Cl₂ / 20 °C

10.1: 93 percent / NaH; TBAI / dimethylformamide / 20 °C

With sodium tetrahydroborate; cerium(III) chloride; acetic anhydride; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; potassium carbonate; ozone; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; xylene; 4.1: Overman rearrangement;
DOI:10.1055/s-2004-837223

Reference yield:

: 57466-98-5
(Z)-ethyl 2-((3aR,5S,6aR)-5-((R)-2,2-dimethyl-1,3-dioxolan-4-yl)-2,2-dimethylfuro[2,3-d][1,3]dioxol-6(3aH,5H,6aH)-ylidene)acetate

: 850359-86-3
C₂₂H₂₉NO₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: 99 percent / DIBALH / CH₂Cl₂ / -20 °C

2.1: DBU / CH₂Cl₂ / -78 °C

3.1: K₂CO₃ / xylene / Heating

4.1: O₃ / CH₂Cl₂ / -78 °C

4.2: 90 percent / Et₃N / CH₂Cl₂ / 0 °C

5.1: 95 percent / tetrahydrofuran / 0 °C

6.1: 96 percent / DMSO; Ac₂O / 20 °C

7.1: 70 percent / NaBH₄; CeCl₃*7H₂O / CH₂Cl₂; methanol / -10 °C

8.1: 99 percent / DBU / CH₂Cl₂ / 20 °C

9.1: 93 percent / NaH; TBAI / dimethylformamide / 20 °C

With sodium tetrahydroborate; cerium(III) chloride; acetic anhydride; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; potassium carbonate; ozone; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; xylene; 3.1: Overman rearrangement;
DOI:10.1055/s-2004-837223