Technology Process of C34H32N8O
There total 11 articles about C34H32N8O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran;
DOI:10.1021/ja991714g
- Guidance literature:
-
Multi-step reaction with 11 steps
1: 92 percent / Me3Al / toluene / 20 °C
2: 87 percent / NaH / dimethylformamide
3: 70 percent / BCl3 / -78 °C
4: 80 percent / camphorsulfonic acid monohydrate
5: 90 percent / (Ph3P)2PdCl2; Et3N / N,N-dimethyl-acetamide / 100 °C
6: camphorsulfonic acid monohydrate / tetrahydrofuran
7: NaBH4 / methanol
8: Pb(OAc)4 / benzene
9: NaBH4 / methanol
10: sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran / Heating
11: (PhO)2P(O)N3; Ph3P; diethyl azodicarboxylate / tetrahydrofuran
With
lead(IV) acetate; bis-triphenylphosphine-palladium(II) chloride; sodium tetrahydroborate; diphenyl phosphoryl azide; camphor-10-sulfonic acid; trimethylaluminum; boron trichloride; sodium hydride; triethylamine; triphenylphosphine; sodium bis(2-methoxyethoxy)aluminium dihydride; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; N,N-dimethyl acetamide; N,N-dimethyl-formamide; toluene; benzene;
1: Condensation / 2: N-benzylation / 3: debenzylation / 4: Condensation / 5: Cyclization / 6: Hydrolysis / 7: Reduction / 8: Ring cleavage / 9: Reduction / 10: Reduction / 11: azidation; Mitsunobu reaction;
DOI:10.1021/ja991714g
- Guidance literature:
-
Multi-step reaction with 3 steps
1: NaBH4 / methanol
2: sodium bis(2-methoxyethoxy)aluminum hydride / tetrahydrofuran / Heating
3: (PhO)2P(O)N3; Ph3P; diethyl azodicarboxylate / tetrahydrofuran
With
sodium tetrahydroborate; diphenyl phosphoryl azide; triphenylphosphine; sodium bis(2-methoxyethoxy)aluminium dihydride; diethylazodicarboxylate;
In
tetrahydrofuran; methanol;
1: Reduction / 2: Reduction / 3: azidation; Mitsunobu reaction;
DOI:10.1021/ja991714g