2-((6-chloropyridin-3-yl)methoxy)-N-(4-nitrophenylcarbamothioyl)benzamide

Base Information

Chemical Name:2-((6-chloropyridin-3-yl)methoxy)-N-(4-nitrophenylcarbamothioyl)benzamide
CAS No.:1402209-26-0
Molecular Formula:C₂₀H₁₅ClN₄O₄S
Molecular Weight:442.882
Hs Code.:

Synonyms:2-((6-chloropyridin-3-yl)methoxy)-N-(4-nitrophenylcarbamothioyl)benzamide

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Chemical Property of 2-((6-chloropyridin-3-yl)methoxy)-N-(4-nitrophenylcarbamothioyl)benzamide

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Technology Process of 2-((6-chloropyridin-3-yl)methoxy)-N-(4-nitrophenylcarbamothioyl)benzamide

There total 6 articles about 2-((6-chloropyridin-3-yl)methoxy)-N-(4-nitrophenylcarbamothioyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₁₄H₉ClN₂O₂S

: 100-01-6,104810-17-5
4-nitro-aniline

: 1402209-26-0
2-((6-chloropyridin-3-yl)methoxy)-N-(4-nitrophenylcarbamothioyl)benzamide

Guidance literature:: In acetonitrile; at 60 - 70 ℃; for 3h;
DOI:10.2174/15701808113109990045

Reference yield:

: 1402209-28-2
2-((6-chloropyridin-3-yl)methoxy)benzoic acid

: 1402209-26-0
2-((6-chloropyridin-3-yl)methoxy)-N-(4-nitrophenylcarbamothioyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 4 - 6 h / Reflux

2: acetonitrile / 1 - 2 h / 60 - 70 °C

3: acetonitrile / 0.5 - 3 h / 60 - 70 °C

With thionyl chloride; In acetonitrile;
DOI:10.1016/j.saa.2012.04.102

Reference yield:

: 1402209-29-3
methyl 2-((6-chloropyridin-3-yl)methoxy)benzoate

: 1402209-26-0
2-((6-chloropyridin-3-yl)methoxy)-N-(4-nitrophenylcarbamothioyl)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; water / methanol / 4 - 6 h / 45 - 50 °C

2: thionyl chloride / 4 - 6 h / Reflux

3: acetonitrile / 1 - 2 h / 60 - 70 °C

4: acetonitrile / 0.5 - 3 h / 60 - 70 °C

With thionyl chloride; water; sodium hydroxide; In methanol; acetonitrile;
DOI:10.1016/j.saa.2012.04.102