8-(1-methylethyl)-4-(N-methyl-N-phenylamino)-2-(methylsulfanyl)pyrazolo[1,5-a]-1,3,5-triazine

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Chemical Name:8-(1-methylethyl)-4-(N-methyl-N-phenylamino)-2-(methylsulfanyl)pyrazolo[1,5-a]-1,3,5-triazine
CAS No.:1099104-60-5
Molecular Formula:C₁₆H₁₉N₅S
Molecular Weight:313.426
Hs Code.:

Synonyms:8-(1-methylethyl)-4-(N-methyl-N-phenylamino)-2-(methylsulfanyl)pyrazolo[1,5-a]-1,3,5-triazine

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Chemical Property of 8-(1-methylethyl)-4-(N-methyl-N-phenylamino)-2-(methylsulfanyl)pyrazolo[1,5-a]-1,3,5-triazine

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Technology Process of 8-(1-methylethyl)-4-(N-methyl-N-phenylamino)-2-(methylsulfanyl)pyrazolo[1,5-a]-1,3,5-triazine

There total 2 articles about 8-(1-methylethyl)-4-(N-methyl-N-phenylamino)-2-(methylsulfanyl)pyrazolo[1,5-a]-1,3,5-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 8-acetyl-4-(N-methyl-N-phenylamino)-2-(methylsulfanyl)pyrazolo[1,5-a]-1,3,5-triazine

: 75-16-1
methylmagnesium bromide

: 1099104-60-5
8-(1-methylethyl)-4-(N-methyl-N-phenylamino)-2-(methylsulfanyl)pyrazolo[1,5-a]-1,3,5-triazine

Guidance literature:: 8-acetyl-4-(N-methyl-N-phenylamino)-2-(methylsulfanyl)pyrazolo[1,5-a]-1,3,5-triazine; methylmagnesium bromide; In tetrahydrofuran; ethanol; at 0 - 20 ℃;

With sodium tetrahydroborate; trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm801340z

Reference yield:

: C₁₆H₁₉N₅OS

: 1099104-60-5
8-(1-methylethyl)-4-(N-methyl-N-phenylamino)-2-(methylsulfanyl)pyrazolo[1,5-a]-1,3,5-triazine

Guidance literature:: C₁₆H₁₉N₅OS; With sodium tetrahydroborate; trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

With sodium hydroxide; water; In dichloromethane;
DOI:10.1016/j.bmc.2009.03.007