2-dimethylaminoacetyl-2'-methyl-4'-(N'-butyl-p-toluenesulfonamido)aniline

Base Information

Chemical Name:2-dimethylaminoacetyl-2'-methyl-4'-(N'-butyl-p-toluenesulfonamido)aniline
CAS No.:83473-50-1
Molecular Formula:C₂₂H₃₁N₃O₃S
Molecular Weight:417.572
Hs Code.:

Synonyms:2-dimethylaminoacetyl-2'-methyl-4'-(N'-butyl-p-toluenesulfonamido)aniline

Suppliers and Price of 2-dimethylaminoacetyl-2'-methyl-4'-(N'-butyl-p-toluenesulfonamido)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-dimethylaminoacetyl-2'-methyl-4'-(N'-butyl-p-toluenesulfonamido)aniline

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-dimethylaminoacetyl-2'-methyl-4'-(N'-butyl-p-toluenesulfonamido)aniline

There total 5 articles about 2-dimethylaminoacetyl-2'-methyl-4'-(N'-butyl-p-toluenesulfonamido)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 109-65-9
1-bromo-butane

: 83473-35-2
2-dimethylaminoacetyl-2'-methyl-4'-(p-toluenesulfonamido)aniline

: 83473-50-1
2-dimethylaminoacetyl-2'-methyl-4'-(N'-butyl-p-toluenesulfonamido)aniline

Guidance literature:: With potassium carbonate; In acetone; for 168h; Ambient temperature;
DOI:10.1002/jps.2600710619

Reference yield:

: 83473-10-3
2-chloro-N-(2-methyl-4-nitrophenyl)acetamide

: 83473-50-1
2-dimethylaminoacetyl-2'-methyl-4'-(N'-butyl-p-toluenesulfonamido)aniline

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / NaHCO₃ / benzene / 30 h / Heating

2: 95 percent / Fe, conc. HCl / ethanol; H₂O / 0.58 h / Heating

3: 90 percent / pyridine / CH₂Cl₂ / 0 - 5 °C

4: 79 percent / K₂CO₃ / acetone / 168 h / Ambient temperature

With pyridine; hydrogenchloride; iron; sodium hydrogencarbonate; potassium carbonate; In ethanol; dichloromethane; water; acetone; benzene;
DOI:10.1002/jps.2600710619

Reference yield:

: 83473-61-4
2-dimethylaminoacetyl-2'-methyl-4'-aminoanilide

: 83473-50-1
2-dimethylaminoacetyl-2'-methyl-4'-(N'-butyl-p-toluenesulfonamido)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine / CH₂Cl₂ / 0 - 5 °C

2: 79 percent / K₂CO₃ / acetone / 168 h / Ambient temperature

With pyridine; potassium carbonate; In dichloromethane; acetone;
DOI:10.1002/jps.2600710619