N-Benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-seryl-L-leucin-2-iodethylester

Base Information

Chemical Name:N-Benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-seryl-L-leucin-2-iodethylester
CAS No.:89017-95-8
Molecular Formula:C₅₃H₅₃IN₂O₁₅
Molecular Weight:1084.91
Hs Code.:

Synonyms:N-Benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-seryl-L-leucin-2-iodethylester

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Chemical Property of N-Benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-seryl-L-leucin-2-iodethylester

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Technology Process of N-Benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-seryl-L-leucin-2-iodethylester

There total 9 articles about N-Benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-seryl-L-leucin-2-iodethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 88962-64-5
N-Benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-seryl-L-leucin-2-bromethylester

: 89017-95-8
N-Benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-seryl-L-leucin-2-iodethylester

Guidance literature:: With sodium iodide; In acetone; for 15h; Ambient temperature;

Reference yield:

: 14218-11-2
2,3,4,6-tetra-O-benzoylglucosyl bromide

: 89017-95-8
N-Benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-seryl-L-leucin-2-iodethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / silver triflate, tetramethyl urea / CH₂Cl₂ / 1) 3-4 h, -30 deg C, 2) 2-3 d, room temperature

2: 90 percent / NaI / acetone / 15 h / Ambient temperature

With silver trifluoromethanesulfonate; tetramethylurea; sodium iodide; In dichloromethane; acetone;

Reference yield:

: 61-90-5,21675-61-6,25248-98-0,70-45-1
L-leucine

: 89017-95-8
N-Benzyloxycarbonyl-O-(2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl)-L-seryl-L-leucin-2-iodethylester

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / thionylchloride / 40 - 50 °C

2: 88 percent / dicyclohexylcarbodiimide, N-hydroxysuccinimide, triethylamine

3: 27 percent / silver triflate, tetramethyl urea / CH₂Cl₂ / 1) 3-4 h, -30 deg C, 2) 2-3 d, room temperature

4: 90 percent / NaI / acetone / 15 h / Ambient temperature

With 1-hydroxy-pyrrolidine-2,5-dione; thionyl chloride; silver trifluoromethanesulfonate; triethylamine; dicyclohexyl-carbodiimide; tetramethylurea; sodium iodide; In dichloromethane; acetone;