C₆₄H₉₀N₄O₁₂Si₃

Base Information

Chemical Name:C₆₄H₉₀N₄O₁₂Si₃
CAS No.:1334176-55-4
Molecular Formula:C₆₄H₉₀N₄O₁₂Si₃
Molecular Weight:1191.69
Hs Code.:

C<sub>64</sub>H<sub>90</sub>N<sub>4</sub>O<sub>12</sub>Si<sub>3</sub>

Synonyms:C₆₄H₉₀N₄O₁₂Si₃

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Chemical Property of C₆₄H₉₀N₄O₁₂Si₃

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Technology Process of C₆₄H₉₀N₄O₁₂Si₃

There total 9 articles about C₆₄H₉₀N₄O₁₂Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1334176-54-3
C₄₈H₇₂N₄O₁₂Si₂

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1334176-55-4
C₆₄H₉₀N₄O₁₂Si₃

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 36h; Inert atmosphere;
DOI:10.1002/chem.201101821

Reference yield:

: 1334176-53-2
N⁽³⁾-benzyloxymethyl-3',5'-O-di(triethylsilyl)-5,6-dihydrothymidine

: 1334176-55-4
C₆₄H₉₀N₄O₁₂Si₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: pyridine hydrogenfluoride / acetonitrile / 4 h / -20 °C / Inert atmosphere

3.1: 1H-imidazole / N,N-dimethyl-formamide / 36 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; pyridine hydrogenfluoride; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201101821

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1334176-55-4
C₆₄H₉₀N₄O₁₂Si₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / Inert atmosphere

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Reflux; Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

5.1: pyridine hydrogenfluoride / acetonitrile / 4 h / -20 °C / Inert atmosphere

6.1: 1H-imidazole / N,N-dimethyl-formamide / 36 h / 0 - 20 °C / Inert atmosphere

With 1H-imidazole; N-Bromosuccinimide; pyridine hydrogenfluoride; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/chem.201101821