rac-1-bromo-4-(3,4-dimethoxybenzyl)-4,5,6,7-tetrahydrothieno[3,4-c]pyridine

Base Information

Chemical Name:rac-1-bromo-4-(3,4-dimethoxybenzyl)-4,5,6,7-tetrahydrothieno[3,4-c]pyridine
CAS No.:1394174-88-9
Molecular Formula:C₁₆H₁₈BrNO₂S
Molecular Weight:368.294
Hs Code.:

Synonyms:rac-1-bromo-4-(3,4-dimethoxybenzyl)-4,5,6,7-tetrahydrothieno[3,4-c]pyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-1-bromo-4-(3,4-dimethoxybenzyl)-4,5,6,7-tetrahydrothieno[3,4-c]pyridine

Chemical Property:

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Technology Process of rac-1-bromo-4-(3,4-dimethoxybenzyl)-4,5,6,7-tetrahydrothieno[3,4-c]pyridine

There total 4 articles about rac-1-bromo-4-(3,4-dimethoxybenzyl)-4,5,6,7-tetrahydrothieno[3,4-c]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1394174-90-3
C₁₆H₁₆BrNO₂S

: 1394174-88-9
rac-1-bromo-4-(3,4-dimethoxybenzyl)-4,5,6,7-tetrahydrothieno[3,4-c]pyridine

Guidance literature:: With methanol; sodium tetrahydroborate; at 0 ℃;

Reference yield:

: 893421-71-1
2-(2-bromothiophen-3-yl)ethylamine

: 1394174-88-9
rac-1-bromo-4-(3,4-dimethoxybenzyl)-4,5,6,7-tetrahydrothieno[3,4-c]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.08 h

1.2: 6 h

2.1: dmap; trifluoromethylsulfonic anhydride / dichloromethane / 0 °C

2.2: 0 °C

3.1: sodium tetrahydroborate; methanol / 0 °C

With methanol; dmap; sodium tetrahydroborate; trifluoromethylsulfonic anhydride; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1394174-89-0
N-[2-(2-bromothiophen-3-yl)ethyl]-2-(3,4-dimethoxyphenyl)acetamide

: 1394174-88-9
rac-1-bromo-4-(3,4-dimethoxybenzyl)-4,5,6,7-tetrahydrothieno[3,4-c]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; trifluoromethylsulfonic anhydride / dichloromethane / 0 °C

1.2: 0 °C

2.1: sodium tetrahydroborate; methanol / 0 °C

With methanol; dmap; sodium tetrahydroborate; trifluoromethylsulfonic anhydride; In dichloromethane;