benzyl benzo[d]oxazol-2-ylcarbamate

Base Information

Chemical Name:benzyl benzo[d]oxazol-2-ylcarbamate
CAS No.:105485-21-0
Molecular Formula:C₁₅H₁₂N₂O₃
Molecular Weight:268.272
Hs Code.:

Synonyms:benzyl benzo[d]oxazol-2-ylcarbamate

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Chemical Property of benzyl benzo[d]oxazol-2-ylcarbamate

Chemical Property:

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Technology Process of benzyl benzo[d]oxazol-2-ylcarbamate

There total 4 articles about benzyl benzo[d]oxazol-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: benzyl (bis(chloro)methylene)carbamate

: 95-55-6
2-amino-phenol

: 105485-21-0
benzyl benzo[d]oxazol-2-ylcarbamate

Guidance literature:: With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2015.09.076

Reference yield:

: benzyl (bis(methylthio)methylene)carbamate

: 105485-21-0
benzyl benzo[d]oxazol-2-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: chlorine / dichloromethane; tetrachloromethane / 0.5 h / -78 °C

2: potassium carbonate / tetrahydrofuran / 1 h / 20 °C

With chlorine; potassium carbonate; In tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1016/j.tetlet.2015.09.076

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 105485-21-0
benzyl benzo[d]oxazol-2-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 4-methyl-morpholine / tetrahydrofuran / -78 °C

2: chlorine / dichloromethane; tetrachloromethane / 0.5 h / -78 °C

3: potassium carbonate / tetrahydrofuran / 1 h / 20 °C

With 4-methyl-morpholine; chlorine; potassium carbonate; In tetrahydrofuran; tetrachloromethane; dichloromethane;
DOI:10.1016/j.tetlet.2015.09.076