p-tolylethynyl germatrane

Base Information

Chemical Name:p-tolylethynyl germatrane
CAS No.:489433-01-4
Molecular Formula:C₁₅H₁₉GeNO₃
Molecular Weight:333.911
Hs Code.:

Synonyms:p-tolylethynyl germatrane

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Chemical Property of p-tolylethynyl germatrane

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Technology Process of p-tolylethynyl germatrane

There total 1 articles about p-tolylethynyl germatrane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 102-71-6,64114-46-1
triethanolamine

: 10038-98-9
germaniumtetrachloride

: 766-97-2
4-n-methylphenylacetylene

: 489433-01-4
p-tolylethynyl germatrane

Guidance literature:: With Et₃N; EtOH; In ethanol; toluene; (N2); standard Schlenk technique; flask with mixt. of CH3C6H4CCH, GeCl4,Et3N in toluene was sealed, cooled, evacuated; heated at 110°C f or 21 h; filtered; residue washed (toluene); EtOH and Et3N were added tofiltrate and washings; mixt. stirred; at room temp. for 50 min; filtered; residue washed (toluene); filtrate and washings were added to (HOCH2CH2)3N; mixt. was stirred at 110°C for 6 h; cooled to room temp.; filtered; washed (pentane; CH2Cl2); solvent removed (vac.); elem. anal.;
DOI:10.1021/om020578c