C₃₅H₃₈N₂O₅S

Base Information

Chemical Name:C₃₅H₃₈N₂O₅S
CAS No.:1340498-75-0
Molecular Formula:C₃₅H₃₈N₂O₅S
Molecular Weight:598.763
Hs Code.:

C<sub>35</sub>H<sub>38</sub>N<sub>2</sub>O<sub>5</sub>S

Synonyms:C₃₅H₃₈N₂O₅S

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Chemical Property of C₃₅H₃₈N₂O₅S

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Technology Process of C₃₅H₃₈N₂O₅S

There total 3 articles about C₃₅H₃₈N₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 122224-36-6
1-N-(4,4'-dimethoxytrithyl)-D(+)-biotin methyl ester

: 106-96-7
propargyl bromide

: 1340498-75-0
C₃₅H₃₈N₂O₅S

Guidance literature:: 1-N-(4,4'-dimethoxytrithyl)-D(+)-biotin methyl ester; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; for 0.25h; Inert atmosphere; Cooling with ice;

propargyl bromide; With tetra-(n-butyl)ammonium iodide; In N,N-dimethyl-formamide; toluene; mineral oil; at 20 ℃; for 3h; regioselective reaction; Cooling with ice; Inert atmosphere;
DOI:10.1021/jo201615j

Reference yield:

: 58-85-5,22879-79-4
biotin

: 1340498-75-0
C₃₅H₃₈N₂O₅S

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride

2.1: pyridine; dmap; triethylamine / 4 h / 75 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / Inert atmosphere; Cooling with ice

3.2: 3 h / 20 °C / Cooling with ice; Inert atmosphere

With pyridine; dmap; thionyl chloride; sodium hydride; triethylamine; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo201615j

Reference yield:

: 608-16-2
biotin methyl ester

: 1340498-75-0
C₃₅H₃₈N₂O₅S

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; dmap; triethylamine / 4 h / 75 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / Inert atmosphere; Cooling with ice

2.2: 3 h / 20 °C / Cooling with ice; Inert atmosphere

With pyridine; dmap; sodium hydride; triethylamine; In N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo201615j