8-mesityl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Base Information

• Chemical Name: 8-mesityl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene
• CAS No.: 870753-29-0
• Molecular Formula: C₁₈H₁₇BF₂N₂
• Molecular Weight: 310.154
• Mol file: 870753-29-0.mol

Synonyms:8-mesityl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property of 8-mesityl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 8-mesityl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

There total 4 articles about 8-mesityl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

mesityl dipyrromethane (382138-81-0) + trifluoroborane diethyl ether (109-63-7) → 8-mesityl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (870753-29-0)

Guidance literature:

With triethylamine; In dichloromethane; at room temp. for 30 min with 10 equiv. of triethylamine; flash chromy.;

DOI:10.1021/jp0525078

Reference yield: 40.0%

boron trifluoride diethyl etherate (109-63-7) + 5-(mesityl)dipyrromethane (159152-14-4) → 8-mesityl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (870753-29-0)

Guidance literature:

5-(mesityl)dipyrromethane; With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h;

boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1039/d0cc08163a

Reference yield:

mesityl dipyrromethane (382138-81-0) → 8-mesityl-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene (870753-29-0)

Guidance literature:

With boron trifluoride diethyl etherate; triethylamine; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1002/ejoc.201100736

upstream raw materials:

mesityl dipyrromethane

trifluoroborane diethyl ether

5-(mesityl)dipyrromethane

boron trifluoride diethyl etherate

Downstream raw materials:

C₁₉H₁₇BF₂N₂O