8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(S)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(S)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside
CAS No.:900180-52-1
Molecular Formula:C₃₆H₄₈Cl₃N₄O₁₅P
Molecular Weight:914.128
Hs Code.:

8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(S)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside

Synonyms:8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(S)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside

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Chemical Property of 8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(S)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside

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Technology Process of 8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(S)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside

There total 7 articles about 8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(S)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 900180-46-3
8-azido-3,6-dioxaoctyl 3-O-benzyl-β-D-galactopyranosyl-(1->3)-2-acetamido-6-O-benzyl-2-deoxy-β-D-glucopyranoside

: 18868-46-7
2,2,2-trichloroethyl phosphorodichloridate

: 900180-52-1
8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(S)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside

: 900180-47-4
8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(R)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; at -15 ℃;
DOI:10.1016/j.carres.2006.04.007

Reference yield:

: 900180-45-2
8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-(β-D-galactopyranosyl)-β-D-glucopyranoside

: 900180-52-1
8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(S)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: Bu₂SnO / toluene / Heating

1.2: 80 percent / CsF / dimethylformamide / 20 °C

2.1: 18 percent / pyridine / CH₂Cl₂ / -15 °C

With pyridine; di(n-butyl)tin oxide; In dichloromethane; toluene;
DOI:10.1016/j.carres.2006.04.007

Reference yield:

: 900180-44-1
8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-2-deoxy-3-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-glucopyranoside

: 900180-52-1
8-azido-3,6-dioxaoctyl 2-acetamido-6-O-benzyl-3-O-(3-O-benzyl-β-D-galactopyranosyl-(S)-P-4,6-cyclic 2,2,2-trichloroethyl phosphate)-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: 96 percent / K₂CO₃ / methanol / 20 °C

2.1: Bu₂SnO / toluene / Heating

2.2: 80 percent / CsF / dimethylformamide / 20 °C

3.1: 18 percent / pyridine / CH₂Cl₂ / -15 °C

With pyridine; di(n-butyl)tin oxide; potassium carbonate; In methanol; dichloromethane; toluene;
DOI:10.1016/j.carres.2006.04.007