2-<(4R,6S)-6-(2-benzyloxy-1,1-dimethylethyl)-2,2-dimethyl-1,3-dioxan-4-yl>ethanol

Base Information

Chemical Name:2-<(4R,6S)-6-(2-benzyloxy-1,1-dimethylethyl)-2,2-dimethyl-1,3-dioxan-4-yl>ethanol
CAS No.:121352-95-2
Molecular Formula:C₁₉H₃₀O₄
Molecular Weight:322.445
Hs Code.:

Synonyms:2-<(4R,6S)-6-(2-benzyloxy-1,1-dimethylethyl)-2,2-dimethyl-1,3-dioxan-4-yl>ethanol

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Chemical Property of 2-<(4R,6S)-6-(2-benzyloxy-1,1-dimethylethyl)-2,2-dimethyl-1,3-dioxan-4-yl>ethanol

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Technology Process of 2-<(4R,6S)-6-(2-benzyloxy-1,1-dimethylethyl)-2,2-dimethyl-1,3-dioxan-4-yl>ethanol

There total 24 articles about 2-<(4R,6S)-6-(2-benzyloxy-1,1-dimethylethyl)-2,2-dimethyl-1,3-dioxan-4-yl>ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 121352-94-1
2,2-Dimethyl-propionic acid 2-[(4R,6S)-6-(2-benzyloxy-1,1-dimethyl-ethyl)-2,2-dimethyl-[1,3]dioxan-4-yl]-ethyl ester

: 121352-95-2
2-<(4R,6S)-6-(2-benzyloxy-1,1-dimethylethyl)-2,2-dimethyl-1,3-dioxan-4-yl>ethanol

Guidance literature:: With diisobutylaluminium hydride; In diethyl ether; hexane; at -78 ℃; for 1h;
DOI:10.1021/jo00273a009

Reference yield:

: 224968-30-3
[(4S,6S)-6-(2-Benzyloxy-1,1-dimethyl-ethyl)-2,2-dimethyl-[1,3]dioxan-4-yl]-acetic acid phenyl ester

: 121352-95-2
2-<(4R,6S)-6-(2-benzyloxy-1,1-dimethylethyl)-2,2-dimethyl-1,3-dioxan-4-yl>ethanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; Yield given; Ambient temperature;
DOI:10.1021/ja990031y

Reference yield:

: 77-76-9
2,2-dimethoxy-propane

: 121352-95-2
2-<(4R,6S)-6-(2-benzyloxy-1,1-dimethylethyl)-2,2-dimethyl-1,3-dioxan-4-yl>ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 9 mg / camphorsulfonic acid, 70 percent hydrogen fluoride-pyridine / CH₂Cl₂ / 0.5 h

2: LiAlH₄ / tetrahydrofuran / 1 h / Ambient temperature

With lithium aluminium tetrahydride; camphor-10-sulfonic acid; pyridine hydrogenfluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja990031y