1-(10,11-Dihydro-dibenzo[b,f]thiepin-10-yl)-4-((E)-3-phenyl-allyl)-piperazine; compound with oxalic acid

Base Information

Chemical Name:1-(10,11-Dihydro-dibenzo[b,f]thiepin-10-yl)-4-((E)-3-phenyl-allyl)-piperazine; compound with oxalic acid
CAS No.:139305-20-7
Molecular Formula:C₂H₂O₄*C₂₇H₂₈N₂S
Molecular Weight:502.634
Hs Code.:

Synonyms:1-(10,11-Dihydro-dibenzo[b,f]thiepin-10-yl)-4-((E)-3-phenyl-allyl)-piperazine; compound with oxalic acid

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Chemical Property of 1-(10,11-Dihydro-dibenzo[b,f]thiepin-10-yl)-4-((E)-3-phenyl-allyl)-piperazine; compound with oxalic acid

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Technology Process of 1-(10,11-Dihydro-dibenzo[b,f]thiepin-10-yl)-4-((E)-3-phenyl-allyl)-piperazine; compound with oxalic acid

There total 3 articles about 1-(10,11-Dihydro-dibenzo[b,f]thiepin-10-yl)-4-((E)-3-phenyl-allyl)-piperazine; compound with oxalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 1725-32-2
10-chloro-10,11-dihydro-dibenzo[b,f]thiepine

: 18903-01-0,114312-65-1,87179-40-6
trans-1-cinnamylpiperazine

: 139305-20-7
1-(10,11-Dihydro-dibenzo[b,f]thiepin-10-yl)-4-((E)-3-phenyl-allyl)-piperazine; compound with oxalic acid

Guidance literature:: In dichloromethane; for 1h; Ambient temperature;
DOI:10.1248/cpb.39.2564

Reference yield:

: 1527-20-4
10,11-Dihydrodibenzothiepin-10-ol

: 139305-20-7
1-(10,11-Dihydro-dibenzo[b,f]thiepin-10-yl)-4-((E)-3-phenyl-allyl)-piperazine; compound with oxalic acid

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 0.17 h / Ambient temperature

2: 13 percent / CH₂Cl₂ / 1 h / Ambient temperature

With thionyl chloride; In dichloromethane;
DOI:10.1248/cpb.39.2564

Reference yield:

: 1898-85-7
dibenzo[b,f]thiepin-10(11H)-one

: 139305-20-7
1-(10,11-Dihydro-dibenzo[b,f]thiepin-10-yl)-4-((E)-3-phenyl-allyl)-piperazine; compound with oxalic acid

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / methanol / 0.33 h / 0 °C

2: SOCl₂ / 0.17 h / Ambient temperature

3: 13 percent / CH₂Cl₂ / 1 h / Ambient temperature

With sodium tetrahydroborate; thionyl chloride; In methanol; dichloromethane;
DOI:10.1248/cpb.39.2564