Ethyl 3-(3,4-bis(benzyloxy)phenyl)-2-(1,3-dioxoisoindolin-2-yl) propanoate

Base Information

Chemical Name:Ethyl 3-(3,4-bis(benzyloxy)phenyl)-2-(1,3-dioxoisoindolin-2-yl) propanoate
CAS No.:128217-67-4
Molecular Formula:C₃₃H₂₉NO₆
Molecular Weight:535.596
Hs Code.:

Synonyms:Ethyl 3-(3,4-bis(benzyloxy)phenyl)-2-(1,3-dioxoisoindolin-2-yl) propanoate

Suppliers and Price of Ethyl 3-(3,4-bis(benzyloxy)phenyl)-2-(1,3-dioxoisoindolin-2-yl) propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 3-(3,4-bis(benzyloxy)phenyl)-2-(1,3-dioxoisoindolin-2-yl) propanoate

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Technology Process of Ethyl 3-(3,4-bis(benzyloxy)phenyl)-2-(1,3-dioxoisoindolin-2-yl) propanoate

There total 10 articles about Ethyl 3-(3,4-bis(benzyloxy)phenyl)-2-(1,3-dioxoisoindolin-2-yl) propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22509-74-6
N-ethoxycarbonylphthalimide

: 128217-67-4,128299-82-1
3-(3,4-Bis-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃ / H₂O; tetrahydrofuran / overnight

2: SOCl₂ / 48 h / Ambient temperature

3: K₂CO₃, NaI / ethanol / 4 h / Heating

With thionyl chloride; sodium hydrogencarbonate; potassium carbonate; sodium iodide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jo00301a008

Reference yield:

: 59-92-7,90638-38-3
3,4-dihydroxy-L-phenylalanine

: 128217-67-4,128299-82-1
3-(3,4-Bis-benzyloxy-phenyl)-2-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 48 h / Ambient temperature

2: NaHCO₃ / H₂O; tetrahydrofuran / overnight

3: K₂CO₃, NaI / ethanol / 4 h / Heating

With thionyl chloride; sodium hydrogencarbonate; potassium carbonate; sodium iodide; In tetrahydrofuran; ethanol; water;
DOI:10.1021/jo00301a008