C₂₂H₁₈F₄N₂O₃

Base Information

Chemical Name:C₂₂H₁₈F₄N₂O₃
CAS No.:1276040-22-2
Molecular Formula:C₂₂H₁₈F₄N₂O₃
Molecular Weight:434.39
Hs Code.:

C<sub>22</sub>H<sub>18</sub>F<sub>4</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₂H₁₈F₄N₂O₃

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Chemical Property of C₂₂H₁₈F₄N₂O₃

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Technology Process of C₂₂H₁₈F₄N₂O₃

There total 5 articles about C₂₂H₁₈F₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65753-52-8
2-fluoro-3-trifluoromethylpyridine

: C₁₆H₁₇NO₃

: 1276040-22-2
C₂₂H₁₈F₄N₂O₃

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 85 ℃;

Reference yield:

: 124700-41-0
2-fluoro-5-iodobenzoic acid

: 1276040-22-2
C₂₂H₁₈F₄N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide; acetonitrile / 20 °C

2.1: bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 2 h / Reflux

3.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

4.1: potassium carbonate / dimethyl sulfoxide / 70 °C

4.2: 2 h / 70 °C

4.3: 6 h / 2 °C

5.1: potassium carbonate / dimethyl sulfoxide / 85 °C

With sodium periodate; osmium(VIII) oxide; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;

Reference yield:

: 625471-27-4
methyl 2-fluoro-5-iodo-benzoate

: 1276040-22-2
C₂₂H₁₈F₄N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 2 h / Reflux

2.1: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

3.1: potassium carbonate / dimethyl sulfoxide / 70 °C

3.2: 2 h / 70 °C

3.3: 6 h / 2 °C

4.1: potassium carbonate / dimethyl sulfoxide / 85 °C

With sodium periodate; osmium(VIII) oxide; potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; water; dimethyl sulfoxide; tert-butyl alcohol;