4-benzyl-3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide

Base Information

Chemical Name:4-benzyl-3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide
CAS No.:1305270-76-1
Molecular Formula:C₂₈H₂₅N₃O₄S
Molecular Weight:499.59
Hs Code.:

Synonyms:4-benzyl-3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide

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Chemical Property of 4-benzyl-3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide

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Technology Process of 4-benzyl-3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide

There total 3 articles about 4-benzyl-3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1305267-26-8
3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide

: 100-39-0
benzyl bromide

: 1305270-76-1
4-benzyl-3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide

Guidance literature:: 3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide; With sodium hydride; In tetrahydrofuran; mineral oil; for 0.25h;

benzyl bromide; In tetrahydrofuran; mineral oil; at 20 ℃; for 3h;

Reference yield:

: 69099-31-6
5,5-dioxo-1-phenyl-4,5-dihydro-1H-5λ⁶-thiochromeno[4,3-c]pyrazole-3-carboxylic acid

: 1305270-76-1
4-benzyl-3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0.5 h / 20 °C

2.1: dichloromethane / 0.5 h / 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h

3.2: 3 h / 20 °C

With oxalyl dichloride; sodium hydride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; mineral oil;

Reference yield:

: C₁₇H₁₁ClN₂O₃S

: 1305270-76-1
4-benzyl-3-(morpholin-4-ylcarbonyl)-1-phenyl-1,4-dihydrothiochromeno[4,3-c]pyrazole 5,5-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 0.5 h / 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h

2.2: 3 h / 20 °C

With sodium hydride; In tetrahydrofuran; dichloromethane; mineral oil;