3-<2-(2-t-butyldiphenylsilyloxyethyl)-4,5-dimethoxyphenyl>-6,7-dimethoxytetrahydroisoquinoline

Base Information

Chemical Name:3-<2-(2-t-butyldiphenylsilyloxyethyl)-4,5-dimethoxyphenyl>-6,7-dimethoxytetrahydroisoquinoline
CAS No.:173031-04-4
Molecular Formula:C₃₇H₄₅NO₅Si
Molecular Weight:611.854
Hs Code.:

Synonyms:3-<2-(2-t-butyldiphenylsilyloxyethyl)-4,5-dimethoxyphenyl>-6,7-dimethoxytetrahydroisoquinoline

Suppliers and Price of 3-<2-(2-t-butyldiphenylsilyloxyethyl)-4,5-dimethoxyphenyl>-6,7-dimethoxytetrahydroisoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<2-(2-t-butyldiphenylsilyloxyethyl)-4,5-dimethoxyphenyl>-6,7-dimethoxytetrahydroisoquinoline

Chemical Property:

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Technology Process of 3-<2-(2-t-butyldiphenylsilyloxyethyl)-4,5-dimethoxyphenyl>-6,7-dimethoxytetrahydroisoquinoline

There total 2 articles about 3-<2-(2-t-butyldiphenylsilyloxyethyl)-4,5-dimethoxyphenyl>-6,7-dimethoxytetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1026632-82-5
[1-{2-[2-(tert-Butyl-diphenyl-silanyloxy)-ethyl]-4,5-dimethoxy-phenyl}-2-(3,4-dimethoxy-phenyl)-ethyl]-methoxymethyl-amine

: 173031-04-4
3-<2-(2-t-butyldiphenylsilyloxyethyl)-4,5-dimethoxyphenyl>-6,7-dimethoxytetrahydroisoquinoline

Guidance literature:: With titanium tetrachloride; In dichloromethane; for 1h; Yield given; -78 deg C to r.t.;
DOI:10.1016/0040-4020(95)00770-9

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 173030-97-2
1-<2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-4,5-dimethoxyphenyl>-2-(3,4-dimethoxyphenyl)ethylamine

: 173031-04-4
3-<2-(2-t-butyldiphenylsilyloxyethyl)-4,5-dimethoxyphenyl>-6,7-dimethoxytetrahydroisoquinoline

Guidance literature:: With titanium tetrachloride; Product distribution; 1.) methanol, reflux, 1 h, 2.) CH₂Cl₂, -78 deg C to r.t., 1 h; mild cyclization method for further N-methoxymethy-N-1,2-diarylethylamines;
DOI:10.1016/0040-4020(95)00770-9