Technology Process of C23H40O4Si
There total 11 articles about C23H40O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine; trifluoroacetic anhydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1016/j.tetasy.2013.07.011
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / methanol / 0.5 h / 20 °C
2: manganese(IV) oxide / dichloromethane / 4 h / Reflux
3: BHA / toluene / 3 h / 80 °C / Inert atmosphere
4: trifluoroacetic anhydride; triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
With
manganese(IV) oxide; triethylamine; trifluoroacetic anhydride; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.tetasy.2013.07.011
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine / 2 h / 20 °C
2: 1H-imidazole; dmap / tetrahydrofuran / 3 h / 60 °C / Inert atmosphere
3: sodium hydroxide / methanol / 0.5 h / 20 °C
4: manganese(IV) oxide / dichloromethane / 4 h / Reflux
5: BHA / toluene / 3 h / 80 °C / Inert atmosphere
6: trifluoroacetic anhydride; triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere
With
pyridine; 1H-imidazole; dmap; manganese(IV) oxide; triethylamine; trifluoroacetic anhydride; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.tetasy.2013.07.011