4'-hydroxy-2,2',4-tribromodiphenyl ether

Base Information

Chemical Name:4'-hydroxy-2,2',4-tribromodiphenyl ether
CAS No.:602326-21-6
Molecular Formula:C₁₂H₇Br₃O₂
Molecular Weight:422.898
Hs Code.:

Synonyms:4'-hydroxy-2,2',4-tribromodiphenyl ether

Suppliers and Price of 4'-hydroxy-2,2',4-tribromodiphenyl ether

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 6 raw suppliers

Chemical Property of 4'-hydroxy-2,2',4-tribromodiphenyl ether

Chemical Property:

Purity/Quality:: 99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 4'-hydroxy-2,2',4-tribromodiphenyl ether

There total 2 articles about 4'-hydroxy-2,2',4-tribromodiphenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 602326-20-5
3-bromo-4-(2,4-dibromophenoxy)benzaldehyde

: 602326-21-6
4'-hydroxy-2,2',4-tribromodiphenyl ether

Guidance literature:: 3-bromo-4-(2,4-dibromophenoxy)benzaldehyde; With potassium dihydrogenphosphate; trifluoroacetyl peroxide; In dichloromethane; at 0 ℃; for 1.5h;

With hydrogenchloride; In methanol; for 15h; Further stages.;
DOI:10.1002/ejoc.200300081

Reference yield:

: 77771-02-9
3-bromo-4-fluorobenzaldehyde

: 602326-21-6
4'-hydroxy-2,2',4-tribromodiphenyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: 78 percent / Na₂CO₃ / N,N-dimethyl-acetamide / 2 h / Heating

2.1: KH₂PO₄; CF₃CO₃H / CH₂Cl₂ / 1.5 h / 0 °C

2.2: 95 percent / hydrochloric acid / methanol / 15 h

With potassium dihydrogenphosphate; trifluoroacetyl peroxide; sodium carbonate; In dichloromethane; N,N-dimethyl acetamide; 2.1: Baeyer-Villiger oxidation;
DOI:10.1002/ejoc.200300081

Reference yield: 99.0%

: 602326-21-6
4'-hydroxy-2,2',4-tribromodiphenyl ether

: 74-88-4
methyl iodide

: 4'-methoxy-2,2',4-tribromodiphenyl ether

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydroxide; In dichloromethane; water; at 20 ℃; for 5h;
DOI:10.1002/ejoc.200300081