2-aminophenyl 6-chloro-7-hydroxycoumarin-4-acetamidophenyl phosphoric acid

Base Information

Chemical Name:2-aminophenyl 6-chloro-7-hydroxycoumarin-4-acetamidophenyl phosphoric acid
CAS No.:407578-86-3
Molecular Formula:C₂₃H₁₈ClN₂O₈P
Molecular Weight:516.831
Hs Code.:

Synonyms:2-aminophenyl 6-chloro-7-hydroxycoumarin-4-acetamidophenyl phosphoric acid

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Chemical Property of 2-aminophenyl 6-chloro-7-hydroxycoumarin-4-acetamidophenyl phosphoric acid

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Technology Process of 2-aminophenyl 6-chloro-7-hydroxycoumarin-4-acetamidophenyl phosphoric acid

There total 2 articles about 2-aminophenyl 6-chloro-7-hydroxycoumarin-4-acetamidophenyl phosphoric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.9%

: 72304-21-3
6-chloro-7-hydroxycoumarin-4-acetic acid

: 407578-85-2
bis(4-aminophenyl)phosphoric acid

: 407578-86-3
2-aminophenyl 6-chloro-7-hydroxycoumarin-4-acetamidophenyl phosphoric acid

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 ℃;
DOI:10.1021/ja011251q

Reference yield:

: 645-15-8
Bis(p-nitrophenyl) phosphate

: 407578-86-3
2-aminophenyl 6-chloro-7-hydroxycoumarin-4-acetamidophenyl phosphoric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / H₂ / 10percent Pd/C / ethanol; H₂O / 3 h

2: 8.9 percent / DIEA; EDC*HCl; HOBt / dimethylformamide / 0 °C

With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; 10percent Pd/C; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ja011251q