2(1H)-Pyridone, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)-

Base Information

Chemical Name:2(1H)-Pyridone, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)-
CAS No.:22969-05-7
Molecular Formula:C10H13 N O4
Molecular Weight:211.21
Hs Code.:2934999090
NSC Number:144747
DSSTox Substance ID:DTXSID70945671
Mol file:22969-05-7.mol

Synonyms:22969-05-7;1-(2-deoxypentofuranosyl)pyridin-2(1h)-one;NSC144747;DTXSID70945671;DQZGJGMNLCTHMX-UHFFFAOYSA-N;2(1H)-Pyridinone, 1-(2-deoxy-.beta.-D-erythro-pentofuranosyl)-;2(1H)-Pyridone, 1-(2-deoxy-.beta.-D-erythro-pentofuranosyl)-;NSC-144747;2(1H)-Pyridone, 1-(2-deoxy-.alpha.-D-erythro-pentofuranosyl)-

Suppliers and Price of 2(1H)-Pyridone, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2(1H)-Pyridone, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)-

Chemical Property:

Vapor Pressure:5.23E-13mmHg at 25°C
Boiling Point:520.5°C at 760 mmHg
Flash Point:268.6°C
PSA：71.69000
Density:1.412g/cm³
LogP:-0.51100
XLogP3:-0.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:211.08445790
Heavy Atom Count:15
Complexity:313

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(C(OC1N2C=CC=CC2=O)CO)O

Technology Process of 2(1H)-Pyridone, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)-

There total 11 articles about 2(1H)-Pyridone, 1-(2-deoxy-beta-D-erythro-pentofuranosyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 24617-00-3
1-<2'-deoxy-3',5'-di-O-(p-toluoyl)-β-D-erythro-pentofuranosyl>-2(1H)-pyridone

: 22969-05-7
1-(4-hydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)pyridin-2-one

Guidance literature:: With ammonia; In methanol; for 24h; Ambient temperature;

Reference yield: 73.0%

: (3-acetoxy-5-(2-oxo-1-pyridyl)tetrahydrofuran-2-yl)methyl acetate

: 22969-05-7
1-(4-hydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)pyridin-2-one

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 0.333333h;
DOI:10.1080/15257770.2015.1122197

Reference yield:

: 142-08-5,1199357-22-6
2-Pyridone

: 22969-05-7
1-(4-hydroxy-5-(hydroxymethyl)tetrahydrofuran-2-yl)pyridin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: bis-TMS acetamide / acetonitrile / 1.17 h

1.2: SnCl₄ / acetonitrile; CH₂Cl₂ / 0 - 20 °C

2.1: NaOMe / methanol / 0.33 h / 20 °C

With sodium methylate; N,N-bis(trimethylsilyl)acetamide; In methanol; acetonitrile;
DOI:10.1002/anie.200601272