benzyl-[3-(benzyl-benzyloxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid benzyl ester

Base Information

Chemical Name:benzyl-[3-(benzyl-benzyloxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid benzyl ester
CAS No.:253591-01-4
Molecular Formula:C₃₉H₃₆N₂O₅S
Molecular Weight:644.791
Hs Code.:

Synonyms:benzyl-[3-(benzyl-benzyloxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid benzyl ester

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Chemical Property of benzyl-[3-(benzyl-benzyloxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid benzyl ester

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Technology Process of benzyl-[3-(benzyl-benzyloxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid benzyl ester

There total 7 articles about benzyl-[3-(benzyl-benzyloxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1212-08-4
S-Phenyl benzenethiosulfonate

: 253590-82-8
benzyl-[3-(benzyl-benzyloxycarbonyl-amino)-2-oxo-propyl]-carbamic acid benzyl ester

: 253591-01-4
benzyl-[3-(benzyl-benzyloxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid benzyl ester

Guidance literature:: With n-butyllithium; In 1,2-dichloro-ethane; at -25 - 20 ℃; for 1h;
DOI:10.1016/S0223-5234(00)80031-8

Reference yield:

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 253591-01-4
benzyl-[3-(benzyl-benzyloxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 20 °C

2: 85 percent / NaOCl; sat. NaHCO₃; KBr / TEMPO / CH₂Cl₂; H₂O / 0 - 20 °C

3: 40 percent / nBuLi / 1,2-dichloro-ethane / 1 h / -25 - 20 °C

With sodium hypochlorite; n-butyllithium; sodium hydrogencarbonate; potassium bromide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; In dichloromethane; water; 1,2-dichloro-ethane; 1: Carboxylation / 2: Oxidation / 3: Substitution;
DOI:10.1016/S0223-5234(00)80031-8

Reference yield:

: 100-52-7
benzaldehyde

: 253591-01-4
benzyl-[3-(benzyl-benzyloxycarbonyl-amino)-2-oxo-3-phenylsulfanyl-propyl]-carbamic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: Na₂SO₄ / CH₂Cl₂ / 20 °C

2: NaBH₄ / ethanol / 20 °C

3: CH₂Cl₂ / 20 °C

4: 85 percent / NaOCl; sat. NaHCO₃; KBr / TEMPO / CH₂Cl₂; H₂O / 0 - 20 °C

5: 40 percent / nBuLi / 1,2-dichloro-ethane / 1 h / -25 - 20 °C

With sodium hypochlorite; sodium tetrahydroborate; n-butyllithium; sodium hydrogencarbonate; sodium sulfate; potassium bromide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; In ethanol; dichloromethane; water; 1,2-dichloro-ethane; 1: Condensation / 2: Reduction / 3: Carboxylation / 4: Oxidation / 5: Substitution;
DOI:10.1016/S0223-5234(00)80031-8