2,3,4,6-tetra-O-acetyl-1-S-(Z)-4-methoxybenzohydroximoyl-1-thio-β-D-glucopyranose

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-1-S-(Z)-4-methoxybenzohydroximoyl-1-thio-β-D-glucopyranose
CAS No.:160280-01-3
Molecular Formula:C₂₂H₂₇NO₁₁S
Molecular Weight:513.522
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetyl-1-S-(Z)-4-methoxybenzohydroximoyl-1-thio-β-D-glucopyranose

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Chemical Property of 2,3,4,6-tetra-O-acetyl-1-S-(Z)-4-methoxybenzohydroximoyl-1-thio-β-D-glucopyranose

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Technology Process of 2,3,4,6-tetra-O-acetyl-1-S-(Z)-4-methoxybenzohydroximoyl-1-thio-β-D-glucopyranose

There total 2 articles about 2,3,4,6-tetra-O-acetyl-1-S-(Z)-4-methoxybenzohydroximoyl-1-thio-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 19879-84-6
tetraacetyl thioglucose

: 38435-51-7
N-hydroxy-4-methoxy-benzenecarboximidoyl chloride

: 160280-01-3
2,3,4,6-tetra-O-acetyl-1-S-(Z)-4-methoxybenzohydroximoyl-1-thio-β-D-glucopyranose

Guidance literature:: With triethylamine; In diethyl ether; dichloromethane; for 1h; Ambient temperature;
DOI:10.1080/00397919408011744

Reference yield:

: 3717-21-3,3717-22-4,140461-28-5,140461-29-6,3235-04-9
p-methoxyl benzaldoxime

: 160280-01-3
2,3,4,6-tetra-O-acetyl-1-S-(Z)-4-methoxybenzohydroximoyl-1-thio-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine, N-chlorosuccinimide / CHCl₃ / 2 h / Ambient temperature

2: 71 percent / NEt₃ / diethyl ether; CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; N-chloro-succinimide; triethylamine; In diethyl ether; dichloromethane; chloroform;
DOI:10.1080/00397919408011744