Technology Process of ethyl 2,4-dimethoxy-6-pentylbenzoate
There total 1 articles about ethyl 2,4-dimethoxy-6-pentylbenzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Aethylolivetolcarboxylat(14), K2CO3, 2 Me2SO4;
- Guidance literature:
-
With
tin(IV) chloride;
In
dichloromethane;
for 2h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 84 percent / SnCl4 / CH2Cl2 / 2 h / Ambient temperature
2: 92 percent / BCl3 / CH2Cl2 / 0.5 h / -78 °C
3: 53 percent / sodium / 20 h / 120 - 130 °C
4: 82 percent / K2CO3 / acetone / 20 h / Heating
5: m-chloroperbenzoic acid / CH2Cl2 / 1 h / Ambient temperature
6: 10percent aq. KOH / methanol / 0.75 h / 0 °C
7: H2 / 10percent Pd/C / ethyl acetate / 16 h
8: diethyl ether / 2 h / Ambient temperature
9: 73 percent / trifluoroacetic anhydride / toluene / 2 h / Ambient temperature
10: 32 percent / K2CO3 / dimethylsulfoxide / 22 h / 75 - 76 °C
With
potassium hydroxide; hydrogen; sodium; boron trichloride; tin(IV) chloride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride;
palladium on activated charcoal;
In
methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; ethyl acetate; acetone; toluene;
