[1,3-bis(3,5-di-t-butylphenyl)ferrocen-2-yl]dichlorostibine

Base Information

• Chemical Name: [1,3-bis(3,5-di-t-butylphenyl)ferrocen-2-yl]dichlorostibine
• CAS No.: 1458219-29-8
• Molecular Formula: C₃₈H₄₉Cl₂FeSb
• Molecular Weight: 754.31
• Mol file: 1458219-29-8.mol

Synonyms:[1,3-bis(3,5-di-t-butylphenyl)ferrocen-2-yl]dichlorostibine

Chemical Property of [1,3-bis(3,5-di-t-butylphenyl)ferrocen-2-yl]dichlorostibine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of [1,3-bis(3,5-di-t-butylphenyl)ferrocen-2-yl]dichlorostibine

There total 1 articles about [1,3-bis(3,5-di-t-butylphenyl)ferrocen-2-yl]dichlorostibine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

1,3-bis(3,5-di-t-butylphenyl)-2-iodoferrocene (1458219-28-7) + antimony(III) chloride (10025-91-9) → [1,3-bis(3,5-di-t-butylphenyl)ferrocen-2-yl]dichlorostibine (1458219-29-8)

Guidance literature:

1,3-bis(3,5-di-t-butylphenyl)-2-iodoferrocene; With tert.-butyl lithium; In diethyl ether; pentane; at -78 - 20 ℃; for 1.5h; Inert atmosphere;

antimony(III) chloride; In diethyl ether; pentane; at -78 - 20 ℃; for 13h; Inert atmosphere;

DOI:10.1246/bcsj.20130174

Reference yield: 44.0%

[1,3-bis(3,5-di-t-butylphenyl)ferrocen-2-yl]dichlorostibine (1458219-29-8) → 1,2-bis[1,3-bis(3,5-di-t-butylphenyl)ferrocen-2-yl]distibene

Guidance literature:

With magnesium; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1246/bcsj.20130174

upstream raw materials:

1,3-bis(3,5-di-t-butylphenyl)-2-iodoferrocene

antimony(III) chloride