ethylzinc diphenylamide

Base Information

• Chemical Name: ethylzinc diphenylamide
• CAS No.: 1730-61-6
• Molecular Formula: C₁₄H₁₅NZn
• Molecular Weight: 262.67
• Mol file: 1730-61-6.mol

Synonyms:ethylzinc diphenylamide

Chemical Property of ethylzinc diphenylamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of ethylzinc diphenylamide

There total 1 articles about ethylzinc diphenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ ethylzinc diphenylamide (1730-61-6)

Guidance literature:

Diaethylzink , Diphenylamin;

DOI:10.1016/S0022-328X(00)86197-5

Reference yield: 48.0%

carbon dioxide (124-38-9,18923-20-1) + cyclohexane-1,2-epoxide (286-20-4) + ethylzinc diphenylamide (1730-61-6) → 2-hydroxycyclohexyl diphenylcarbamate

Guidance literature:

In benzene; at 80 ℃; for 120h; under 38000 Torr;

DOI:10.1246/bcsj.61.2913

Reference yield:

2,2-dimethyl-3-pentanone (564-04-5) + ethylzinc diphenylamide (1730-61-6) → (CH3)3CC(OZnC2H5)CHCH3 (109930-68-9) + diphenylamine (122-39-4)

Guidance literature:

In benzene-d6; equimolar quantities of starting materials, room temp., 69 h, under N2; equil. reaction, t-BuC(OZnEt)=CHMe to t-BuC(O)Et ratio 1:1 ((1)H NMR data);

DOI:10.1021/om00153a006

Downstream raw materials:

N,N-Diphenyl-3-hydroxypropionamid

(CH₃)3CC(OZnC₂H₅)CHCH₃

diphenylamine