1-(((5S,6S,7R,8R,Z)-8,11-bis(tert-butyldimethylsilyloxy)-5,7-dimethylundeca-1,3-dien-6-yloxy)methyl)-4-methoxybenzene

Base Information

Chemical Name:1-(((5S,6S,7R,8R,Z)-8,11-bis(tert-butyldimethylsilyloxy)-5,7-dimethylundeca-1,3-dien-6-yloxy)methyl)-4-methoxybenzene
CAS No.:623926-60-3
Molecular Formula:C₃₃H₆₀O₄Si₂
Molecular Weight:577.008
Hs Code.:

Synonyms:1-(((5S,6S,7R,8R,Z)-8,11-bis(tert-butyldimethylsilyloxy)-5,7-dimethylundeca-1,3-dien-6-yloxy)methyl)-4-methoxybenzene

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Chemical Property of 1-(((5S,6S,7R,8R,Z)-8,11-bis(tert-butyldimethylsilyloxy)-5,7-dimethylundeca-1,3-dien-6-yloxy)methyl)-4-methoxybenzene

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Technology Process of 1-(((5S,6S,7R,8R,Z)-8,11-bis(tert-butyldimethylsilyloxy)-5,7-dimethylundeca-1,3-dien-6-yloxy)methyl)-4-methoxybenzene

There total 15 articles about 1-(((5S,6S,7R,8R,Z)-8,11-bis(tert-butyldimethylsilyloxy)-5,7-dimethylundeca-1,3-dien-6-yloxy)methyl)-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₆H₇₀O₅Si₃

: 623926-60-3
1-(((5S,6S,7R,8R,Z)-8,11-bis(tert-butyldimethylsilyloxy)-5,7-dimethylundeca-1,3-dien-6-yloxy)methyl)-4-methoxybenzene

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1.3h;
DOI:10.1021/jm061385k

Reference yield:

: 1026307-82-3
(2R,3R,4R,5R)-5,8-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-2,4-dimethyl-octanal

: 623926-60-3
1-(((5S,6S,7R,8R,Z)-8,11-bis(tert-butyldimethylsilyloxy)-5,7-dimethylundeca-1,3-dien-6-yloxy)methyl)-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: CrCl₂ / tetrahydrofuran / 17 h / 20 °C

2: 1.85 g / NaH / tetrahydrofuran / 1.3 h / 0 - 20 °C

With chromium dichloride; sodium hydride; In tetrahydrofuran; 1: Nozaki-Hiyama-Kishi reaction / 2: Peterson elimination;
DOI:10.1021/jm061385k